Microencapsuled conjugated linoleic acid glyceride powder and preparation method thereof
AssigneeInnobio Corporation Limited
InventorsXiang Ren, Yutao Xu, Zhongle Tian, Jianbin Chen, Wenzhong Wu
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Abstract
The present invention discloses a microencapsuled conjugated linoleic acid glyceride powder and a preparation method thereof. The preparation method comprises the steps of preparing raw materials, preparing an aqueous phase and an oil phase, preparing an emulsion, and spray drying. The raw materials comprise, in parts by mass: 60-85 parts of conjugated linoleic acid glyceride, 5-35 parts of starch or colloid, 4-20 parts of small molecule filler, and 0.01-5 parts of antioxidant.
Claims7
A method for preparing a microencapsulated conjugated linoleic acid glyceride powder, comprising
- step 1:
- preparing raw materials containing the following components in parts by mass, based on a total mass of the raw materials of 100 parts:
- conjugated linoleic acid glyceride
- 60-85
- parts;
- starch or colloid
- 5-35
- parts;
- micromolecule filler
- 4-20
- parts;
- antioxidant
- 0.01-5
- parts;
- step 2:
- dissolving the starch or the colloid and the micromolecule filler in water at 40° C. to 60° ° C. to form a first mixture, and then cooling the first mixture to 0-30° C.;
- step 3:
- adding an aqueous phase antioxidant into the first mixture in step (2), and stirring at 0° to 30° C. until the aqueous phase antioxidant is completely dissolved in the first mixture to obtain the second mixture;
- step 4:
- adding an oil phase antioxidant into the conjugated linoleic acid glyceride, and stirring at 10-25° C. until the oil phase antioxidant is completely dissolved to obtain an oil phase;
- step 5:
- adding the oil phase into the second mixture to form a third mixture, controlling the temperature of the third mixture between 0-30° C., shearing and emulsifying the third mixture for 0.5 hour to 2 hours, and then homogenizing for 1 time to 3 times at 40-120 MPa to obtain an emulsion;
- and
- step 6:
- performing spray drying on the emulsion prepared in step (5) at an air inlet temperature of 90-230° C., and an air outlet temperature of 50-110° C.,
- wherein the starch comprises native starch or modified starch,
- the modified starch is selected from acid-modified starch, oxidized starch, starch acetate, phosphate acetate, cross-linked starch, hydroxypropyl starch, and pregelatinized starch, and mixtures thereof;
- and
- the colloid is selected from xanthan gum, gelatin, Arabic gum, and mixtures thereof,
- wherein the microsencapsulated conjugated linoleic acid glyceride powder has an embedding rate of 98.1% to 99.5% at an oil load of 70%.
Dependencies are inferred from the claim text.