# US 12,111,330 B2 · Systems and methods for concurrently exposing a test specimen to a first environment and a second environment

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- Number: US 12,111,330 B2
- Document ID: US12111330B2
- Status: Granted
- Kind: B2
- Application number: 17/673,085
- Filed: 2022-02-16
- Published: 2023-08-17
- Granted: 2024-10-08
- Earliest claimed: 2022-02-16
- Assignees: The Boeing Company
- Applicants: The Boeing Company
- Inventors: Bruno Zamorano Senderos; Ali Yousefiani; Austin E. Mann; Michael F. Stoia
- Web page: https://patentgrep.com/patent/US12111330B2

## CPC

- G01N 17/002: {Test chambers}
- G01N 37/00: Details not covered by any other group of this subclass
- B64F 5/60: Testing or inspecting aircraft components or systems
- G01D 21/00: Measuring or testing not otherwise provided for
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)
- B64F: GROUND OR AIRCRAFT-CARRIER-DECK INSTALLATIONS SPECIALLY ADAPTED FOR USE IN CONNECTION WITH AIRCRAFT; DESIGNING, MANUFACTURING, ASSEMBLING, CLEANING, MAINTAINING OR REPAIRING AIRCRAFT, NOT OTHERWISE PROVIDED FOR; HANDLING, TRANSPORTING, TESTING OR INSPECTING AIRCRAFT COMPONENTS, NOT OTHERWISE PROVIDED FOR
- G01D: MEASURING NOT SPECIALLY ADAPTED FOR A SPECIFIC VARIABLE; ARRANGEMENTS FOR MEASURING TWO OR MORE VARIABLES NOT COVERED IN A SINGLE OTHER SUBCLASS; TARIFF METERING APPARATUS; MEASURING OR TESTING NOT OTHERWISE PROVIDED FOR

## Abstract

A material compatibility test design system and method, allowing for the testing of characteristics of behavior of materials in extreme environments, the method including concurrently exposing a test specimen to a first environment and a second environment, the test specimen having an outside surface and an inside surface, the inside surface defining an internal volume, includes exposing the outside surface of the test specimen to the first environment for a predetermined period of time, the first environment comprising a first temperature, a first pressure and a first composition. The method further includes exposing the inside surface of the test specimen to the second environment for a second predetermined period of time, the second environment comprising a second temperature, a second pressure and a second composition.

## Claims

### Claim 1

A method for concurrently exposing a test specimen to a first environment and a second environment, the test specimen comprising an outside surface and an inside surface, the inside surface defining an internal volume, the method comprising:
exposing the outside surface of the test specimen to the first environment for a first predetermined period of time, the first environment comprising a first temperature, a first pressure and a first composition;
exposing the inside surface of the test specimen to the second environment for a second predetermined period of time, the second environment comprising a second temperature, a second pressure and a second composition;
coupling a mechanical load to the test specimen during the exposing the outside surface of the test specimen and the exposing the inside surface of the test specimen;
collecting a sample from the first environment;
qualitative testing the sample from the first environment;
collecting a sample from the second environment; and
qualitative testing the sample from the second environment.

### Claim 2 (depends on 1)

The method of claim 1, wherein the first temperature is about 800° C. to about 1000° C., the first pressure is about 15 psi to about 2500 psi, and the first predetermined period of time is at least 1000 hours.

### Claim 3 (depends on 1)

The method of claim 1, wherein the first environment comprises ambient air.

### Claim 4 (depends on 1)

The method of claim 1, wherein the first environment comprises inert gas.

### Claim 5 (depends on 1)

The method of claim 1, wherein the second temperature is about 800° C. to about 1000° C., wherein the second pressure is about 1500 psi to about 2500 psi, and wherein the second predetermined period of time is at least 1000 hours.

### Claim 6 (depends on 1)

The method of claim 1, wherein the first temperature is different than the second temperature.

### Claim 7 (depends on 1)

The method of claim 1, wherein the first pressure is different than the second pressure.

### Claim 8 (depends on 1)

The method of claim 1, wherein the second environment comprises supercritical carbon dioxide.

### Claim 9 (depends on 1)

The method of claim 1, wherein the first composition is different from the second composition.

### Claim 10 (depends on 1)

The method of claim 1, wherein the test specimen comprises a nickel-based superalloy, a refractory alloy, and a composite material.

### Claim 11 (depends on 1)

The method of claim 1, further comprising:
exposing an outside surface of a second test specimen to the first environment for a predetermined period of time; and
exposing an inside surface of the second test specimen to a third environment for a predetermined period of time, the third environment having a third temperature, a third pressure and a third composition.

### Claim 12 (depends on 11)

The method of claim 11, wherein the exposing the outside surface of the test specimen and the exposing the outside surface of the second test specimen are performed concurrently.

### Claim 13 (depends on 11)

The method of claim 11, wherein the test specimen and the second test specimen are compositionally different.

### Claim 14 (depends on 11)

The method of claim 11, wherein the second composition is different from the third composition.

### Claim 15

A system for testing materials exposed to extreme conditions, the system comprising:
a housing defining a chamber;
a first test specimen received in the chamber, the first test specimen comprising a first outside surface and a first inside surface, the first inside surface defining a first internal volume;
a second test specimen received in the chamber concurrently with the first test specimen, the second test specimen comprising a second outside surface and a second inside surface, the second inside surface defining a second internal volume;
a first fluid source fluidly coupled with the chamber of the housing to supply a first fluid to the chamber, the first fluid having a first composition at a first temperature and a first pressure;
a first pressure control apparatus associated with the first fluid source and configured to control, at least partially, the first pressure of the first fluid;
a second fluid source fluidly couplable with the first internal volume of the first test specimen to supply a second fluid to the first internal volume of the first test specimen, the second fluid having a second composition at a second temperature and a second pressure;
a second pressure control apparatus associated with the second fluid source and configured to control, at least partially, the second pressure of the second fluid;
a third fluid source fluidly couplable with the second internal volume of the second test specimen to supply a second fluid to the second internal volume of the second test specimen, the third fluid having a third composition at a third temperature and a third pressure;
a third pressure control apparatus associated with the third fluid source and configured to control, at least partially, the third pressure of the third fluid; and
a heat source located in the housing, the heat source defining a heated chamber for receiving the first test specimen and the second test specimen, wherein the heated chamber is configured to control, at least partially, the first temperature of the first fluid, the second temperature of the second fluid, and the third temperature of the third fluid.

### Claim 16 (depends on 15)

The system of claim 15, wherein the housing is an autoclave.

### Claim 17 (depends on 15)

The system of claim 15, wherein the first internal volume comprises supercritical carbon dioxide.

### Claim 18 (depends on 15)

The system of claim 15, wherein the first test specimen is tapered.

### Claim 19

A method for testing materials exposed to extreme conditions using a first test specimen and a second test specimen, the first test specimen comprising a first outside surface and a first inside surface, the first inside surface defining a first internal volume, the second test specimen comprising a second outside surface and a second inside surface, the second inside surface defining a second internal volume, the method comprising:
exposing the first outside surface of the first test specimen to a first environment, the first environment comprising a first temperature, a first pressure and a first composition;
exposing the first inside surface of the first test specimen to a second environment, the second environment comprising a second temperature, a second pressure and a second composition;
exposing the second outside surface of the second test specimen to the first environment; and
exposing the second inside surface of the second test specimen to a third environment, the third environment comprising a third temperature, a third pressure and a third composition,
wherein the exposing the first outside surface, the exposing the first inside surface, the exposing the second outside surface, and the exposing the second inside surface are performed concurrently.

### Claim 20 (depends on 15)

The method of claim 15, wherein the second environment comprises supercritical carbon dioxide.