# US 12,111,230 B2 · Thermal gas inspection of plugged honeycomb body > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 12,111,230 B2 - Document ID: US12111230B2 - Status: Granted - Kind: B2 - Application number: 17/434,071 - Filed: 2020-02-20 - Published: 2022-05-05 - Granted: 2024-10-08 - Earliest claimed: 2019-03-14 - Assignees: Corning Incorporated - Applicants: Corning Incorporated - Inventors: Joseph Henry Citriniti; Seungcheol Yang - Web page: https://patentgrep.com/patent/US12111230B2 ## CPC - G01M 3/002: {by using thermal means} - G01N 15/082: {Investigating permeability by forcing a fluid through a sample} - G01N 25/72: Investigating presence of flaws - G01N 2015/084: {Testing filters} - G01M: TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR - G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q) ## Abstract Improved inspection techniques are described herein for identifying leaks in a plugged honeycomb body. The improved inspection techniques utilize a pore impediment and a test gas. The pore impediment is injected into the plugged honeycomb body, and the test gas is forced into the plugged honeycomb body. A thermal detector is used to collect thermal data from an inspection region of an outlet end of the plugged honeycomb body, and the thermal data is used to identify defects in the plugged honeycomb body. ## Claims ### Claim 1 An apparatus to detect leaks in a plugged honeycomb body having a plurality of intersecting porous walls defining a first channel open at a first end of the honeycomb body and plugged at a second end opposite to the first end, and a second channel open at the second end and plugged at the first end, the apparatus comprising: a pore impediment injector configured to inject a pore impediment into a plurality of pores of the intersecting porous walls of the plugged honeycomb body, the pore impediment having an impediment size that is smaller than a mean pore size of the plurality of pores; a gas conditioning device configured to adjust a temperature of a gas to a second temperature; a gas supply configured to force gas from the gas conditioning device into an opening of the first channel at the first end of the plugged honeycomb body, the plugged honeycomb body being at a first temperature that is different from the second temperature of the gas being forced into the opening of the first channel at the first end of the honeycomb body by the gas supply; a thermal detector configured to collect thermal data from an inspection region of the second channel at the second end of the plugged honeycomb body; and one or more processors configured to calculate gradient data related to at least one of a temperature change over time or a temperature difference over space from the thermal data. ### Claim 2 (depends on 1) The apparatus of claim 1, wherein the thermal detector defines a detection axis, wherein the second channel defines a longitudinal axis, and wherein an angle between the detection axis and the longitudinal axis of the second channel is in a range between 1° and 90°. ### Claim 3 (depends on 1) The apparatus of claim 1, wherein the one or more processors are configured to compare the gradient data and a predetermined gradient threshold and to provide output data correlating to the comparison. ### Claim 4 (depends on 1) The apparatus of claim 1, wherein the gas is at least one of air, nitrogen, hydrogen, or helium, and wherein the gas has a relative humidity in a range between 2-40%. ### Claim 5 (depends on 1) The apparatus of claim 1, wherein the pore impediment is at least one of nebulized, atomized, or sprayed liquid. ### Claim 6 (depends on 1) The apparatus of claim 1, wherein the impediment size is in a range between 5-80% of the mean pore size of the plurality of pores. ### Claim 7 A method of detecting leaks in a plugged honeycomb body having a plurality of intersecting porous walls defining a first channel open at a first end of the honeycomb body and plugged at a second end opposite to the first end, and a second channel open at the second end and plugged at the first end, the method comprising: injecting a pore impediment into a plurality of pores of the intersecting porous walls of the plugged honeycomb body, the pore impediment having an impediment size that is smaller than a mean pore size of the plurality of pores; forcing gas into an opening of the first channel defined by the plugged honeycomb body, the plugged honeycomb body being at a first temperature and the gas being at a second temperature that is different from the first temperature; collecting thermal data from an inspection region of the second channel at the second end of the plugged honeycomb body using a thermal detector; and analyzing the thermal data to calculate gradient data related to at least one of a temperature change over time or a temperature difference over space of the inspection region to determine whether the plugged honeycomb body has one or more defects. ### Claim 8 (depends on 7) The method of claim 7, wherein the thermal detector is a thermal imaging camera, and wherein the method further comprises: relating a physical dimension of the plugged honeycomb body; and determining at least one of a size or a location of the identified one or more defects based at least in part on the physical dimension of the plugged honeycomb body being correlated to a pixel of the thermal data. ### Claim 9 (depends on 7) The method of claim 7, wherein collecting the thermal data comprises collecting a plurality of subsets of the thermal data at a plurality of respective times over a duration of time, and wherein at least one of the subsets of the thermal data is collected prior to forcing the gas into the opening of the first channel. ### Claim 10 (depends on 7) The method of claim 7, wherein the pore impediment is at least one of nebulized, atomized, or sprayed liquid. ### Claim 11 (depends on 7) The method of claim 7, wherein analyzing the thermal data comprises comparing first gradient data for a first inspection region and second gradient data for a second inspection region, wherein the first inspection region and the second inspection region are disposed at adjacent channels. ### Claim 12 (depends on 7) The method of claim 7, wherein analyzing the thermal data comprises comparing the gradient data and a predetermined gradient threshold and providing output data correlating to the comparison. ### Claim 13 (depends on 12) The method of claim 12, wherein the predetermined gradient threshold is a number of adjacent pixels superimposed over the plugged honeycomb body having a gradient value greater than a predetermined gradient value. ### Claim 14 (depends on 12) The method of claim 12, wherein the predetermined gradient threshold is a number of pixels superimposed over the plugged honeycomb body located within a predetermined radius having a gradient value greater than a predetermined gradient value. ### Claim 15 (depends on 12) The method of claim 12, wherein the predetermined gradient threshold is a number of pixels superimposed over the plugged honeycomb body having a gradient value greater than a predetermined gradient value. ### Claim 16 (depends on 12) The method of claim 12, wherein the predetermined gradient threshold is a proportion of total pixels superimposed on the plugged honeycomb body having a gradient value greater than a predetermined gradient value. ### Claim 17 (depends on 16) The method of claim 16, wherein the proportion of total pixels is in a range of 10%-100% of the total pixel count of an open channel for that honeycomb body. ### Claim 18 (depends on 7) The method of claim 7, wherein the impediment size is in a range between 5-80% of a mean pore size of the plurality of pores. ### Claim 19 (depends on 7) The method of claim 7, wherein the inspection region of the second channel is disposed on at least one wall of the plugged honeycomb body adjacent an opening of the second channel. ### Claim 20 (depends on 7) The method of claim 7, further comprising sorting the plugged honeycomb body based on the determination of whether the plugged honeycomb body has one or more defects.