# US 12,109,542 B2 · Method and generator of producing solvated nanoclusters > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 12,109,542 B2 - Document ID: US12109542B2 - Status: Granted - Kind: B2 - Application number: 18/287,526 - Filed: 2023-04-17 - Published: 2024-08-15 - Granted: 2024-10-08 - Earliest claimed: 2022-04-18 - Applicants: Niall Joseph English - Inventors: Niall Joseph English - Web page: https://patentgrep.com/patent/US12109542B2 ## CPC - B01F 23/2375: for obtaining bubbles with a size below 1 µm - B01F 25/452: characterised by elements provided with orifices or interstitial spaces - B01F 33/05: Mixers using radiation, e.g. magnetic fields or microwaves to mix the material ({B01F23/2133, B01F23/238, B01F23/55,} B01F33/3031, B01F33/3032 take precedence) - B01F: MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING (mixing paints B44D3/06) ## Abstract A system (300), method and generator (301) for producing solvated nanoclusters of a guest substance. The method comprises providing a container (302) containing a plurality of surfaces (304) distributed therein; introducing a solvent (103) within which the solvated nanoclusters are to be generated into the container such that the solvent comes in contact with the surfaces; and distributing a fluid guest substance within the solvent, wherein the plurality of surfaces comprises random packings or structured packings or both, wherein the packings are made of or coated with (i) permanent-magnetic material or (ii) dielectric material that has a quasi-permanent electric charge or dipole polarisation. ## Claims ### Claim 1 A method of producing solvated nanoclusters, the method comprising the following steps: providing a container with a plurality of surfaces distributed therein; introducing a solvent within which the solvated nanoclusters are to be generated into the container such that the solvent comes in contact with the plurality of surfaces; providing a guest substance in fluid form; and distributing the guest substance within the solvent, wherein the plurality of surfaces comprises random packings or structured packings or both, and wherein the packings are made of or coated with either (i) permanent-magnetic material or (ii) dielectric or charged/polarised material that has a quasi-permanent electric charge or dipole polarisation. ### Claim 2 (depends on 1) The method of claim 1, wherein the plurality of surfaces comprise packings made of or coated with permanent-magnetic material to provide a magnetic strength of from about 0.1 T to about 0.5 T. ### Claim 3 (depends on 1) The method of claim 1, wherein the plurality of surfaces comprise packings made of or coated with dielectric or charged/polarised material that has a quasi-permanent electric charge or dipole polarisation to provide a Coulombic field strength in the range of from about 105 V/m to about 107 V/m. ### Claim 4 (depends on 1) The method of claim 1, wherein the packings are coated with solvophobic and/or solvophilic material to provide regions with solvophobic and/or solvophilic character, respectively. ### Claim 5 (depends on 1) The method of claim 1, wherein the plurality of surfaces comprises packings made of permanent-magnetic material and coated with dielectric or charged/polarised material that has a quasi-permanent electric charge or dipole polarisation. ### Claim 6 (depends on 1) The method of claim 1, wherein the plurality of packings comprises packings with a size in the order of from about 15 mm to about 150 mm. ### Claim 7 (depends on 1) The method of claim 1, wherein the method comprises providing and distributing more than one guest substance in fluid form. ### Claim 8 (depends on 7) The method of claim 7, wherein the guest substances to be distributed within the solvent comprise a plurality of liquids. ### Claim 9 (depends on 1) The method of claim 1, wherein least one guest substance comprises a gas. ### Claim 10 (depends on 1) The method of claim 1, wherein at least one guest substance comprises a liquid. ### Claim 11 (depends on 1) The method of claim 1, wherein the plurality of surfaces comprises surfaces coated with an electrically insulating coating. ### Claim 12 (depends on 1) The method of claim 1, wherein the plurality of surfaces comprises structured packings arranged in a parallel configuration. ### Claim 13 (depends on 1) The method of claim 1; wherein the method further comprises the step of cooling the contents of the container. ### Claim 14 (depends on 1) The method of claim 1, wherein the method further comprises agitating the contents of the container. ### Claim 15 (depends on 1) The method of claim 1, wherein the method further comprises the step of releasing the nanoclusters from the solvent by applying an acoustic-sonication or electromagnetic signal to the container or by adding a chemical agent such as a surfactant to the solvent containing the nanoclusters. ### Claim 16 (depends on 1) A generator for producing nanoclusters using the method of claim 1, the generator comprising: the container containing the plurality of surfaces distributed therein, a solvent inlet for introducing solvent into which the solvated nanoclusters are to be generated into the container such that the solvent comes in contact with the surfaces; and a fluid guest medium inlet for introducing a guest substance in fluid form into the container for distribution within the solvent, wherein the plurality of surfaces comprises random packings or structured packings or both, wherein the packings are made of or coated with either (i) permanent-magnetic material or (ii) dielectric material that has a quasi-permanent electric charge or dipole polarisation to emit spatial force distributions which result in the manipulation of the local density and intermolecular bonding arrangements in the solvent molecules to facilitate absorption of the fluid guest medium in the nanoscale by enhancing the de-stabilisation of macroscopic droplets, clusters and bubbles. ### Claim 17 (depends on 16) The generator as claimed in claim 16 further comprising a fluid-solvent turbulence generator. ### Claim 18 (depends on 16) The generator as claimed in claim 16 further comprising an internal electric source located within the container. ### Claim 19 (depends on 16) A system for generating solvated nanoscale features in a liquid, wherein the nanoscale features are gas, liquid or crystallite form and present in amounts beyond thermodynamic solubility, the system comprising a generator as claimed in claim 16 and one or more sensors, wherein the sensors are selected from among a temperature sensor for sensing temperature associated with the contents of the container, a pressure sensor for sensing pressure associated with the generator and one or more pH sensors. ### Claim 20 (depends on 19) The system as claimed in claim 19 further comprising a data-acquisition system for recording the parameters monitored with said sensors at predetermined intervals. ### Claim 21 (depends on 19) The system as claimed in claim 19 further comprising a storage vessel for storing the generated nanoclusters. ### Claim 22 (depends on 19) The system as claimed in claim 19 further comprising a control circuit in communication with the generator and one or more of a gas source for supplying a gas medium, a liquid source for supplying a liquid medium, a vacuum pump and a cooling means for cooling the contents of the container. ### Claim 23 (depends on 1) A method for improving plant growth comprising watering a plant using water containing air and CO2 nanoclusters generated using the method of claim 1, wherein the solvent is water and the fluid guest medium comprises air and carbon dioxide. ### Claim 24 (depends on 1) A method for capture of CO2 and pollutants from flue-gases and air in solvents, the method comprising generating nanoclusters using the method of claim 1, wherein the plurality of surfaces comprise packings made of permanent magnetic material coated with dielectric material that has a quasi-permanent electric charge or dipole polarisation and further coated with a solvophobic coating. ### Claim 25 (depends on 1) A method for capture of gas and water in petroleum, diesel and oil-bio-based fuels, the method comprising generating nanoclusters using the method of claim 1, wherein the solvent is selected from among petroleum, diesel and oil-bio-based fuels and the plurality of surfaces comprise packings made of permanent magnetic material coated with dielectric material that has a quasi-permanent electric charge or dipole polarisation and further coated with solvophilic and hydrophilic coatings.