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US 12,084,537 B2Granted
Petroleum resin, hydrogenated petroleum resin, and production method for hydrogenated petroleum resin
AssigneeIdemitsu Kosan Co., Ltd.
InventorsKiyohiko Yokota, Kenji Kobayashi, Masakatsu Kuroki
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Abstract
The present invention relates to a petroleum resin having the content of a volatile organic compound component of less than 100 wt ppm; and a hydrogenated petroleum resin having the content of a volatile organic compound component of less than 100 wt ppm.
Claims5
A method for producing a hydrogenated petroleum resin comprising:
- a copolymerization reaction step of subjecting a cyclopentadiene-based compound and a vinyl aromatic compound to a copolymerization reaction in the presence of a polymerization solvent;
- a step of performing a removal treatment of a volatile component which is contained in a copolymerization reaction product liquid obtained in the copolymerization reaction step, to obtain a petroleum resin;
- a hydrogenation reaction step of subjecting the petroleum resin to a hydrogenation reaction in the presence of a hydrogenation solvent;
- a step of performing a removal treatment of an unreacted component and a volatile component which are contained in a hydrogenation reaction product liquid obtained in the hydrogenation reaction step, to obtain a hydrogenated petroleum resin concentrate;
- and
- a removal step of a volatile organic compound component by removing a volatile organic compound component from the hydrogenated petroleum resin concentrate, to obtain a hydrogenated petroleum resin containing 6 to 10% by mass of a hydrogenated low-molecular weight material having a molecular weight of 200 to 350,
- wherein the removal step of a volatile organic compound component is constituted of a first step of supplying the hydrogenated petroleum resin into a thin film distillation apparatus, to control the content of the volatile organic compound component to less than 2,000 wt ppm;
- and a second step of supplying the hydrogenated petroleum resin having passed the first step into a nitrogen-stripping apparatus or a steam distillation apparatus, to control the content of the volatile organic compound component to less than 100 wt ppm.
5 more elements
Dependencies are inferred from the claim text.