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US 11,998,014 B1Granted
O-{1-[(3,5-dinitrobenzoyl)amino]propan-2-yl} (4-chlorophenyl)carbamothioate as an eco-friendly insecticidal agent against Spodoptera littoralis (boisd.)
AssigneeKing Faisal University
InventorsHany Mohamed Abd El-Lateef Ahmed, Mai Mostafa Khalaf Ali, Mohamed Gouda, Antar Ahmed Abdelhamid Ahmed, Mohamed A. Gad
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Abstract
Synthesis of a compound O-{1-[(3.5-dinitrobenzoyl)amino]propan-2-yl} (4-chlorophenyl)carbamothioate and its use as an insecticidal agent.
Claims20
A compound having the formula I:
An insecticidally acceptable composition comprising an insecticidally effective amount of a O-{1-[(3,5-dinitrobenzoyl)amino]propan-2-yl} (4-chlorophenyl)carbamothioate compound having the formula I:
- and an insecticidally acceptable carrier.
A method of making a O-{1-[(3,5-dinitrobenzoyl)amino]propan-2-yl} (4-chlorophenyl)carbamothioate compound, the method comprising:
- mixing N-(2-hydroxypropyl)-3,5-dinitrobenzamide with 4-chlorophenyl isothiocyanate to obtain a reaction mixture;
- refluxing the reaction mixture with 1,4-dioxane and (Triethylamine) TEA to obtain a precipitate;
- filtering and recrystallizing the precipitate;
- and
- obtaining the O-{1-[(3,5-dinitrobenzoyl)amino]propan-2-yl} (4-chlorophenyl)carbamothioate compound.
2 more elements
Dependencies are inferred from the claim text.