Method and device for monitoring the mechanochemical activation of metal powders in dynamic electrochemical environment

A device for monitoring mechanochemical activation of metal powders in dynamic electrochemical environment, comprising a casing (7), a rotating mechanism (4), a replaceable material electrode (1), an adjustable electrode holder (2), and an electrochemical cell (5),

• wherein a top of the casing (7) is provided with the rotating mechanism (4), and a bottom of the casing is provided with the electrochemical cell (5);
• the rotating mechanism (4) is detachably connected to an upper end of a first electrode (14) on an upper part of the replaceable material electrode (1) through a connecting piece (41), configured to drive the replaceable material electrode (1) to rotate as a whole;
• the electrochemical cell (5) is provided with the replaceable material electrode (1), a platinum electrode (24), and a reference electrode (23);
• a lower end of the replaceable material electrode (1) is connected to a working metal plate (11);
• the replaceable material electrode (1) extends into the electrochemical cell (5) and is perpendicular to a bottom of the electrochemical cell (5);
• the working metal plate (11) is in contact with liquid and glass beads in the electrochemical cell (5);
• the platinum electrode (24) and the reference electrode (23) are fixed by an adjustable electrode holder (2);
• the adjustable electrode holder (2) is movably arranged on one side of the casing (7) and is capable of being adjusted up and down;
• the replaceable material electrode (1), the reference electrode (23), and the platinum electrode (24) are respectively connected to an electrochemical workstation through a first working electrode conduction circuit (81), a first reference electrode conduction circuit (82), and a first platinum electrode conduction circuit (83).