# US 11,898,408 B2 · System to manage wellbore servicing fluids containing paramagnetic materials

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- Number: US 11,898,408 B2
- Document ID: US11898408B2
- Status: Granted
- Kind: B2
- Application number: 16/960,338
- Filed: 2019-09-09
- Published: 2022-06-23
- Granted: 2024-02-13
- Earliest claimed: 2019-09-09
- Assignees: Halliburton Energy Services, Inc.
- Applicants: Halliburton Energy Services, Inc.
- Inventors: Dale E. Jamison; William W. Shumway
- Web page: https://patentgrep.com/patent/US11898408B2

## CPC

- E21B 21/06: Arrangements for treating drilling fluids outside the borehole
- E21B 21/063: {by separating components}
- E21B 21/062: {by mixing components}
- B03C 1/32: acting on the medium containing the substance being separated, e.g. magneto-gravimetric-, magnetohydrostatic-, or magnetohydrodynamic separation
- E21B: EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- B03C: MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS (separating isotopes B01D59/00; combinations of magnetic or electrostatic separation with separation of solids by other means B03B, B07B)

## Abstract

Systems and methods for separating paramagnetic material in wellbore return fluid. A quadrupole magnet system is disposed along conduit so that a paramagnetic field is symmetrically formed about a central axis of the conduit. A wellbore return fluid containing paramagnetic material is directed through the conduit. The paramagnetic field drives the paramagnetic material outward towards the perimeter of the conduit, thereby concentrating fluid with little or no paramagnetic material along the central axis of the conduit. An outlet is disposed along the flow path of a portion of the concentrated fluid. In some embodiments, the outlet is positioned along the central axis, while in other embodiments, the outlet is positioned along the conduit wall. The paramagnetic material may be weighting material used to prepare drilling mud.

## Claims

### Claim 1

A method for treating working fluids in the oil and gas industry, the method comprising:
combining a working fluid with a paramagnetic material;
introducing the working fluid into a wellbore;
passing the return working fluid through a quadrupole magnetic field;
measuring a magnetic field of the return working fluid;
dynamically adjusting the quadrupole magnetic field to concentrate a first portion of the return working fluid at a first diameter within the conduit; and
utilizing the dynamically adjusted quadrupole magnetic field to concentrate a second portion of the return working fluid at a second diameter within the conduit,
wherein the second diameter is greater than the first diameter;
wherein a magnetic field sensor is located inside the second diameter and another magnetic field sensor is located outside the first diameter; and
wherein the second portion of the return fluid contains a higher density of paramagnetic materials than the first portion.

### Claim 2 (depends on 1)

The method of claim 1, wherein the working fluid is drilling mud and the paramagnetic material is a weighting material.

### Claim 3 (depends on 1)

The method of claim 1, further comprising separating the concentrated paramagnetic materials from the recovered return fluid.

### Claim 4 (depends on 3)

The method of claim 3, further comprising adjusting the strength of the quadrupole magnetic field to adjust the concentration amount of the paramagnetic material separated from the recovered return fluid.

### Claim 5 (depends on 1)

The method of claim 1, wherein the first portion of the return working fluid is concentrated axially along a central axis of a conduit and the second portion of the return working fluid is concentrated along a wall of the conduit.

### Claim 6 (depends on 5)

The method of claim 5, further comprising positioning an inlet along the central axis and directing flow of the first portion into the inlet.

### Claim 7 (depends on 1)

The method of claim 1, wherein mixing comprises mixing a working fluid with a paramagnetic material selected from a group consisting of hematite, awaruite, hematite composites, carbonate coated hematite charged polymers, charged surfactants, charged organic species, and PHPA polymers.

### Claim 8

A magnetic multipole fluid separation system for the oil and gas industry comprising:
a housing assembly having an outer housing and a central insert, wherein the central insert sealingly engages an inner wall of the outer housing and includes at least two cavities around its outer surface extending to an inner diameter of the outer housing, wherein the at least two cavities are covered with a hermetically sealed cover to prevent fluid contamination of the cavities;
a magnetic assembly located in each one of the at least two cavities, wherein each magnetic assembly comprises one or more permanent magnets or one or more electromagnets;
an electronics insert housing connected to the magnetic assembly through electrical ports;
at least two radially extending outer fluid flow passageways adjacent the inner wall of the at least two cavities, wherein the inner surfaces of the at least two radially extending outer fluid flow passageways are coated with a hydrophobic material;
at least one port along a surface of the at least two radially extending outer fluid flow passageways;
an outer exit bore in the central insert comprising fluid exit ports connected to an annulus fluid stream outside of outer housing;
a central conduit; and
a valve to control flow of fluid from central conduit into the at least two radially extending outer fluid flow passageways.

### Claim 9 (depends on 8)

The system of claim 8, wherein the magnetic assembly comprises a quadrupole magnet system having at least four spaced apart magnets positioned symmetrically in the at least two cavities, where opposing magnets have the same polarity and adjacent magnets have the opposite polarity.

### Claim 10 (depends on 9)

The system of claim 9, wherein the magnetic assembly comprises one or more permanent magnets.

### Claim 11 (depends on 8)

The system of claim 8, wherein the magnetic assembly comprises one or more electromagnets.

### Claim 12 (depends on 8)

The system of claim 8, further comprising a central outlet port.

### Claim 13 (depends on 8)

The system of claim 8, wherein the magnetic assembly comprises a plurality of quadrupole magnet.

### Claim 14 (depends on 8)

The system of claim 8, further comprising a magnetic field sensor disposed adjacent the multipole magnet system.

### Claim 15

A magnetic quadrupole fluid separation system for the oil and gas industry comprising:
a first tube disposed along a primary axis and having a first end and a second end;
a second tube having an inlet at a first end, the inlet positioned within the first tube along the primary axis between the first and second ends of the first tube;
a valve to control flow of fluid into the first tube and the second tube, wherein the valve can stop the flow of fluid into the first tube and divert it into the second tube, wherein the valve is constructed from titanium, ceramic, stellite, or tungsten carbide; and
a quadrupole magnet system disposed along the first tube between the first end of the first tube and the first end of the second tube, the quadrupole magnetic system having at least four radially spaced apart magnets positioned symmetrically around the first tube, where opposing magnets have the same polarity and adjacent magnets have the opposite polarity.

### Claim 16 (depends on 15)

The system of claim 15, further comprising a plurality of a quadrupole magnet systems spaced apart axially along a portion of the length of the first tube, each quadrupole magnet system having at least four spaced apart magnets positioned symmetrically around the first tube, where opposing magnets have the same polarity and adjacent magnets have the opposite polarity.

### Claim 17 (depends on 15)

The system of claim 15, further comprising a first quadrupole magnet system having a first magnetic field strength and a second quadrupole magnet system having a second magnetic field strength greater than the first magnetic field strength, the first quadrupole magnet system disposed along the first tube between the first end of the first tube and the first end of the second tube, and the second quadrupole system disposed along a tube downstream of the second tube inlet.

### Claim 18 (depends on 15)

The system of claim 15, wherein the valve comprises a central hub and the valve is attached to a drive member.

### Claim 19 (depends on 15)

The system of claim 15, further comprising an outlet in the first tube adjacent an outer wall of the first tube.

### Claim 20 (depends on 15)

The system of claim 15, wherein the magnets comprise field adjustable electromagnets.