# US 11,896,927 B2 · Radial adsorber with radial circulation of gas

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- Number: US 11,896,927 B2
- Document ID: US11896927B2
- Status: Granted
- Kind: B2
- Application number: 17/683,555
- Filed: 2022-03-01
- Published: 2022-09-08
- Granted: 2024-02-13
- Earliest claimed: 2021-03-05
- Assignees: L'Air Liquide, Societe Anonyme pour l'Etude et l'Exploitation des Procedes Georges Claude
- Applicants: L'Air Liquide, Societe Anonyme pour l'Etude et l'Exploitation des Procedes Georges Claude
- Inventors: Lian-Ming Sun; Christophe Sobre; Christian Monereau; Vincent Gueret
- Web page: https://patentgrep.com/patent/US11896927B2

## CPC

- B01D 53/0431: {Beds with radial gas flow}
- B01J 8/0214: {in a cylindrical annular shaped bed}
- B01D 53/0438: {Cooling or heating systems}
- B01D 53/0446: {Means for feeding or distributing gases}
- B01D 53/0462: {Temperature swing adsorption}
- B01D 53/047: Pressure swing adsorption
- B01D 2259/40: Further details for adsorption processes and devices
- B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28)
- B01J: CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS

## Abstract

A radial adsorber comprising: an adsorbent mass containing particles, a cylindrical shell ring extending along a longitudinal axis that is vertical when the adsorber is in operation, an external grid and an internal grid arranged in such a way as to be permeable to the gas and impermeable to the particles, the internal grid and external grid between them forming an annular volume housing the adsorbent mass, an internal chamber located between the vertical longitudinal axis and the internal grid, an external chamber located between the external grid and the shell ring, the internal chamber and external chamber being intended for the circulation of the gas, the external grid being formed by a plurality of wires and a plurality of supports, the supports being mounted transversely to the wires, the supports and the wires being mounted secured to one another.

## Claims

### Claim 1

A radial adsorber configured for the radial circulation of gas, the radial adsorber comprising:
an adsorbent mass containing particles;
a cylindrical shell ring extending along a longitudinal axis A-A that is vertical when the adsorber is in operation, the shell ring comprising a lower end cap, an upper end cap, and gas inlet/outlet nozzles;
an external grid arranged in such a way as to be permeable to the gas and impermeable to the particles, the external grid extending along the vertical longitudinal axis;
an internal grid arranged in such a way as to be permeable to the gas and impermeable to the particles, the internal grid extending along the vertical longitudinal axis;
sealing means for sealing the lower part and the upper part of the internal grid and external grid, the internal grid and external grid between them forming an annular volume housing the adsorbent mass;
an internal chamber located between the vertical longitudinal axis and the internal grid;
an external chamber located between the external grid and the shell ring, the internal chamber and external chamber being intended for the circulation of the gas;
the external grid being formed by a plurality of wires and a plurality of supports, the supports being mounted transversely to the wires, the supports and the wires being mounted secured to one another, the wires forming a plurality of longitudinal openings for the passage of the gas such that two adjacent wires define one of the longitudinal openings of the plurality, each longitudinal opening having a minimum opening width Lo for the passage of the gas, each wire having, in cross section, a maximum wire width Lf measured in the direction in which the supports extend;
the external grid being arranged in such a way that the supports extend along the vertical longitudinal axis; and
the external grid being arranged in such a way that the supports are positioned on the side of the external chamber and the wires on the side of the adsorbent mass.

### Claim 2 (depends on 1)

The radial adsorber according to claim 1, wherein the external grid is cylindrical, the external grid and the shell ring is concentric.

### Claim 3 (depends on 1)

The radial adsorber according to claim 1, wherein the external chamber defines an annular gas-distribution volume.

### Claim 4 (depends on 1)

The radial adsorber according to claim 1, wherein the external chamber is configured to allow circulation of the gas over an entire periphery of the shell ring without encountering any obstacle.

### Claim 5 (depends on 1)

The radial adsorber according to claim 1, wherein the external grid is configured to satisfy the relationship 0.05<Lo/(Lo+Lf)<0.3.

### Claim 6 (depends on 1)

The radial adsorber according to claim 1, wherein each wire is of flared cross-section and mounted securely to the supports by a narrow end of each wire, a wide end of each wire being left free.

### Claim 7 (depends on 1)

The radial adsorber according to claim 1, wherein the wires and the supports are made of metal and secured to one another by welding at each intersection between a wire and a support.

### Claim 8 (depends on 1)

The radial adsorber according to claim 1, wherein the supports are mounted perpendicular to the wires, the wires being mounted parallel to one another and the supports being mounted parallel to one another.

### Claim 9 (depends on 1)

A gas separation or purification unit comprising at least one radial adsorber according to claim 1, the unit employing a PSA or TSA process.

### Claim 10 (depends on 1)

The gas separation or purification unit according to claim 1, wherein a difference in temperature between a feed stream and a heating stream for regeneration is less than 100° C. when the adsorber is in normal operation.

### Claim 11 (depends on 1)

The gas separation or purification unit according to claim 1, wherein the external grid has an external diameter greater than 2 m and a height greater than or equal to 3 m.
