Method and apparatus for transfer of liquid
AssigneeL'Air Liquide, Societe Anonyme pour l'Etude et l'Exploitation des Procedes Georges Claude
InventorEric Day
Life of this patent
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Abstract
A method and apparatus for transferring a first liquid removed from an outlet of a first distillation column to an inlet of a second distillation column is provided. The second distillation column operates at a higher pressure than the first distillation column, and the inlet of the second distillation column is at higher elevation as compared to the outlet of the first distillation column. The method advantageously transfers the first liquid from the outlet to the inlet by mixing with a sufficient amount of a lower density second liquid that results in a mixed liquid having a reduced density as compared to the first liquid.
Claims10
A method for operating an air separation plant having a higher-pressure column, a lower-pressure column, and an argon column, the air separation plant having a first mode of operation and a second mode of operation, the method comprising the steps of:
- withdrawing an argon-enriched fluid from the lower-pressure column and introducing said argon-enriched fluid to the argon column;
- withdrawing an argon-enriched liquid from a first location of the argon column;
- and
- withdrawing a liquid nitrogen stream from a third location of the higher-pressure column and introducing the liquid nitrogen stream, after expansion in a valve, to a second location of the lower-pressure column, wherein the second location is at a higher elevation than the third location,
- wherein during first mode of operation, the method further comprises the step of sending the argon-enriched liquid withdrawn from the first location of the argon column to a liquid storage tank or to a fourth column configured to further refine the argon-enriched liquid,
- wherein during the second mode of operation, the method further comprises the steps of mixing the argon-enriched liquid from the first location of the argon column with the liquid nitrogen stream at a mixing location that is at a lower elevation than the first location to form a mixed fluid and then introducing the mixed fluid to the second location, wherein the mixed fluid is introduced to the second location without the use of a pump,
- wherein the method is switched from the first mode of operation to the second mode of operation by closing an argon production valve and opening a previously closed second valve for mixing the argon-enriched liquid with the nitrogen-enriched liquid.
A method for operating an air separation plant having a higher-pressure column, a lower-pressure column, and an argon column, the air separation plant having a first mode of operation and a second mode of operation, the method comprising the steps of:
- withdrawing an argon-enriched fluid from the lower-pressure column and introducing said argon-enriched fluid to the argon column;
- withdrawing an argon-enriched liquid from a first location of the argon column;
- and
- withdrawing a liquid nitrogen stream from a third location of the higher-pressure column and introducing the liquid nitrogen stream, after expansion in a valve, to a second location of the lower-pressure column, wherein the second location is at a higher elevation than the third location,
- wherein during first mode of operation, the method further comprises the step of sending the argon-enriched liquid withdrawn from the first location of the argon column to a liquid storage tank or to a fourth column configured to further refine the argon-enriched liquid,
- wherein during the second mode of operation, the method further comprises the steps of mixing the argon-enriched liquid from the first location of the argon column with the liquid nitrogen stream at a mixing location that is at a lower elevation than the first location to form a mixed fluid and then introducing the mixed fluid to the second location, wherein the mixed fluid is introduced to the second location without the use of a pump,
- wherein the step of mixing the argon-enriched liquid further comprises adjusting a flow rate of the argon-enriched liquid being mixed with the liquid nitrogen stream at the mixing location using a second valve,
- wherein the step of mixing the argon-enriched liquid further comprises adjusting a flow rate of the argon-enriched liquid sent from the first location of the argon column to the liquid storage tank or to the fourth column using an argon production valve.
An air separation plant configured to operate in a first mode of operation and a second mode of operation, the apparatus comprising:
- a double column system having a higher-pressure column surmounted by a lower-pressure column, wherein a second location of the lower-pressure column is configured to receive a liquid nitrogen stream from a third location of the higher-pressure column following expansion in a valve;
- an argon production unit in fluid communication with the lower-pressure column, wherein the argon production unit is configured to receive an argon-enriched fluid from the lower-pressure column, wherein the argon production unit is configured to operate at a lower pressure than the lower-pressure column, wherein the argon production unit comprises an argon column and liquid argon storage;
- wherein during first mode of operation, the argon production unit is configured to transfer liquid argon to a liquid storage tank,
- wherein during the second mode of operation, a first location of the argon production unit is configured to be in fluid communication with a mixing location, such that the air separation plant is configured to mix an argon-enriched fluid from the argon production unit with the liquid nitrogen stream from the higher-pressure column at the mixing location, wherein the mixing location is disposed between the second location and the third location, wherein the mixing location is at a lower elevation than the second location and the first location,
- wherein the apparatus further comprises an absence of a pump disposed between the first location and the second location,
- wherein the apparatus is switched from the first mode of operation to the second mode of operation by closing an argon production valve and opening a previously closed mixing valve for mixing the argon-enriched liquid with the nitrogen-enriched liquid.
Dependencies are inferred from the claim text.