Method for producing silica sol having elongated particle shape
AssigneeNissan Chemical Corporation
InventorsSatoru Murakami, Takuya Fukuoka, Kazuya Kuroiwa
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AssigneeNissan Chemical Corporation
InventorsSatoru Murakami, Takuya Fukuoka, Kazuya Kuroiwa
Estimating the term…
A method for producing a silica sol containing a small amount of metal impurities and wherein colloidal silica having an elongated particle shape is dispersed in a solvent, by addition of a compound as an anion source and ammonia as an alkali source and heating of the resultant mixture at a predetermined temperature, includes the following steps: (a) preparing a raw material liquid by adding at least one compound as an anion source selected from the group of inorganic acids, organic acids, and ammonium salts of these acids, and ammonia to a silica sol as a raw material having SiO2 of 1% by mass to 30% by mass and a pH of 2 to 5 so the mass ratio of the compound to SiO2 is 0.5% to 1.9%; and (b) heating the raw material liquid prepared in step (a) at 80° C. to 200° C. for 0.5 hours to 20 hours.
A method for producing a silica sol containing elongated amorphous colloidal silica particles dispersed in a liquid medium and having an SiO2 concentration of 6% by mass to 30% by mass, wherein the silica particles contained in the silica sol exhibit a DL/DB ratio of 2.5 or more and a DL of 30 nm to 300 nm wherein DL is an average particle diameter (nm) as measured by the dynamic light scattering method, and DB is a primary particle diameter (nm) as measured by the nitrogen gas adsorption method, and the silica particles have a particle length of 50 nm to 1,000 nm as determined by observation with an electron microscope, the production method comprising the following steps (a) and (b):
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