Methods of making and using bulk products including fiber-containing particles with dual-tapered shape
AssigneeVartega Inc.
InventorsJordan Gray Harris, Kylie Marie Van Aken, Sean Paul Kline, Andrew Timothy Maxey, Sean Louis Hankins
Life of this patent
Estimating the term…
Abstract
Recycled carbon fibers are processed by rotational tumbling in a mixture with binder material to prepare fiber-containing particles having a dual-tapered shape and general alignment of fibers with a longitudinal direction of the particles. Bulk products including such fiber-containing particles are compounded with polymer and pelletized to prepare fiber-reinforced composite pellets, which are useful for applications such as injection molding to prepare molded products of carbon fiber-reinforced composite material with recycled carbon fibers.
Claims41
A method of making a bulk product comprising a plurality of fiber-containing particles, the method comprising:
- processing a fiber feed and a binder material to prepare fiber-containing particles including fibers from the fiber feed, wherein the fiber feed comprises reinforcing fibers in a non-continuous form and the processing comprises:
- disposing the reinforcing fibers from the fiber feed and the binder material in a process vessel;
- rotational tumbling of a mixture of the reinforcing fibers from the fiber feed and the binder material to form agglomerates each comprising a portion of the reinforcing fibers from the fiber feed and a portion of the binder material, the rotational tumbling comprising rotating the process vessel containing the reinforcing fibers from the fiber feed and the binder material;
- during the rotational tumbling, forming the agglomerates comprising a plurality of dual-tapered agglomerates having a dual-tapered particle structure, wherein the dual-tapered particle structure comprises:
- a particle length dimension, being a maximum separation distance in a longitudinal direction between first and second longitudinal ends of the agglomerate;
- a maximum particle width dimension transverse to the longitudinal direction at a longitudinal location between the first and second longitudinal ends;
- an aspect ratio equal to the particle length dimension divided by the maximum particle width dimension;
- and
- a dual-tapered shape comprising a first tapered portion tapering in the longitudinal direction away from the longitudinal location toward the first longitudinal end and a second tapered portion tapering in the longitudinal direction away from the longitudinal location toward the second longitudinal end;
- and
- recovering the agglomerates including the dual-tapered agglomerates prepared during the rotational tumbling;
- and
- wherein the mixture comprises the binder material in an amount of from 0.5 weight percent to 11 weight percent relative to the weight of the reinforcing fibers from the fiber feed in the mixture.
A method of making a bulk product comprising a plurality of fiber-containing particles, the method comprising:
- processing a fiber feed and a binder material to prepare fiber-containing particles including fibers from the fiber feed, wherein the fiber feed comprises reinforcing fibers in a non-continuous form having a weight average fiber length of the reinforcing fibers in the fiber feed in a range of from 1 millimeter to 18 millimeters;
- the processing comprising rotational tumbling of a mixture of the reinforcing fibers from the fiber feed and the binder material to form agglomerates each comprising a portion of the reinforcing fibers from the fiber feed and a portion of the binder material;
- during the rotational tumbling, forming the agglomerates with at least 25 weight percent of the agglomerates being dual-tapered agglomerates having a dual-tapered particle structure, wherein the dual-tapered particle structure comprises;
- a particle length dimension, being a maximum separation distance in a longitudinal direction between first and second longitudinal ends of the agglomerate;
- a maximum particle width dimension transverse to the longitudinal direction at a longitudinal location between the first and second longitudinal ends;
- an aspect ratio equal to the particle length dimension divided by the maximum particle width dimension;
- and
- a dual-tapered shape comprising a first tapered portion tapering in the longitudinal direction away from the longitudinal location toward the first longitudinal end and a second tapered portion tapering in the longitudinal direction away from the longitudinal location toward the second longitudinal end;
- and
- recovering the agglomerates including the dual-tapered agglomerates prepared during the rotational tumbling;
- wherein the dual-tapered agglomerates comprise:
- from 90 weight percent to 99.5 weight percent reinforcing fibers from the fiber feed;
- and
- from 0.5 weight percent to 10 weight percent of the binder material;
- a weight average particle length dimension in a range of from 3 millimeters to 40 millimeters, wherein the weight average particle length dimension is an average on a weight basis of the particle length dimensions of the dual-tapered agglomerates;
- and
- a weight average aspect ratio of at least 1.5, wherein the weight average aspect ratio is an average on a weight basis of the aspect ratios of the dual-tapered agglomerates.
A method of making a bulk product comprising a plurality of fiber-containing particles, the method comprising:
- processing a fiber feed and a binder material to prepare fiber-containing particles including fibers from the fiber feed, wherein the fiber feed comprises reinforcing fibers in a non-continuous form;
- the processing comprising rotational tumbling of a mixture of the reinforcing fibers from the fiber feed and the binder material to form agglomerates each comprising a portion of the reinforcing fibers from the fiber feed and a portion of the binder material;
- during the rotational tumbling, forming the agglomerates with at least 25 weight percent of the agglomerates being dual-tapered agglomerates having a dual-tapered particle structure;
- wherein the dual-tapered particle structure comprises:
- a particle length dimension, being a maximum separation distance in a longitudinal direction between first and second longitudinal ends of the agglomerate;
- a maximum particle width dimension transverse to the longitudinal direction at a longitudinal location between the first and second longitudinal ends;
- an aspect ratio equal to the particle length dimension divided by the maximum particle width dimension;
- and
- a dual-tapered shape comprising a first tapered portion tapering in the longitudinal direction away from the longitudinal location toward the first longitudinal end and a second tapered portion tapering in the longitudinal direction away from the longitudinal location toward the second longitudinal end;
- recovering the agglomerates including the dual-tapered agglomerates prepared during the rotational tumbling;
- preparing a fiber-containing bulk product comprising a plurality of the fiber-containing particles, the plurality of the fiber-containing particles comprising:
- from 90 weight percent to 99.5 weight percent of the reinforcing fibers from the fiber feed;
- from 0.5 weight percent to 10 weight percent binder, holding the reinforcing fibers in a particle structure;
- each said fiber-containing particle of the plurality of the fiber-containing particles comprising:
- a particle length dimension, being a maximum separation distance in a longitudinal direction between first and second longitudinal ends of the particle;
- a maximum particle width dimension transverse to the longitudinal direction at a longitudinal location between the first and second longitudinal ends;
- an aspect ratio equal to the particle length dimension divided by the maximum particle width dimension;
- and
- a dual-tapered shape comprising a first tapered portion tapering in the longitudinal direction away from the longitudinal location toward the first longitudinal end and a second tapered portion tapering in the longitudinal direction away from the longitudinal location toward the second longitudinal end;
- and
- the plurality of the fiber-containing particles further comprising:
- a weight average particle length dimension of the fiber-containing particles is in a range of from 3 millimeters to 40 millimeters, wherein the weight average particle length dimension is an average on a weight basis of the particle length dimensions of the fiber-containing particles;
- and
- a weight average aspect ratio of the fiber-containing particles of at least 1.5, wherein the weight average aspect ratio is an average on a weight basis of the aspect ratios of the fiber-containing particles;
- wherein the plurality of the fiber-containing particles comprise at least one member selected from the group consisting of the dual-tapered agglomerates and modified dual-tapered particles resulting from subsequent processing of the dual-tapered agglomerates after the rotational tumbling.
Dependencies are inferred from the claim text.