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US 11,767,481 B2Granted
Process for producing biodiesel from acidic raw materials
AssigneePetroleo Brasileiro S.A. - Petrobras
InventorsCristina Pontes Bittencourt Quitete, Felipe Campos Cauby Coutinho, Vitor Loureiro Ximenes
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Abstract
The present invention concerns a process for producing biodiesel with bifunctional heterogeneous acidic catalysts from acidic raw materials, such as fatty acids and mixtures of fatty acids with triglycerides.
Claims5
A process for producing biodiesel from acidic raw materials, characterized in that it comprises:
- a) the use of acidic raw materials and triglycerides in the biodiesel production process;
- b) the integration of the esterification step via acidic and heterogeneous catalysis with the treatment of oils and fats by physical refining and transesterification for the production of biodiesel;
- c) the use of three integration points:
- at the inlet of a first transesterification reactor, at the inlet of a second transesterification reactor and at the inlet of the washing process of the product of the transesterification section;
- d) use of a fixed bed reactor to carry out the esterification step via heterogeneous catalysis;
- e) a transesterification reaction system consisting of three continuous stirred tank reactors in series;
- f) sending the glycerin to a rectifying tower, while the methyl ester is dried and rectified to produce biodiesel;
- and
- g) the methanol-rich stream is rectified to be recycled.
6 more elements
Dependencies are inferred from the claim text.