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US 11,767,474 B2Granted
High temperature bio-char carbonization and micron grinding and classification for inclusion into master batch polymerization
AssigneeThomas Jefferson University
InventorMark Sunderland
Life of this patent
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Abstract
A thermal process for carbonizing hemp and reducing particle size, mechanically, by grinding or milling said carbonized hemp materials to generate a precise particle size hemp char and combining the hemp char particles with a polymer into a master batch.
Claims18
A process for creating a mixture of micron-sized charred hemp comprising:
- rough cutting a portion of hemp stalk said hemp stalk comprising hemp hurd and hemp fibers;
- charring the portion of hemp stalk at a temperature of greater than 1100° C. for a period of at least one hour to create a char material;
- milling the char material by air jet milling, grinding, or ball milling to create a milled char having an irregular polyhedron shape;
- and
- collecting the milled char.
2 more elements
A process for creating a master batch comprising a plurality of hemp char particles and at least one polymer comprising:
- carbonizing a portion of a hemp material, said hemp material comprising hemp hurd and hemp fibers in a furnace, said furnace being flushed with nitrogen and then heated to a temperature of greater than 1100° C.;
- wherein the temperature of greater than 1100° C. is held for at least 60 minutes;
- maintaining nitrogen flow over the at least 60 minutes to maintain a low oxygen environment to create a char;
- removing the char from the furnace and allowing it to cool;
- milling the char by a milling process for a period sufficient to reduce the char into a plurality of char particles having an irregular polyhedron shape by air jet milling or ball milling;
- combining the char particles with the at least one polymer, wherein the ratio of char particles to polymer is between 10:90 and 50:50;
- and
- mixing the at least one polymer and the char particles to form the master batch.
5 more elements
A process of forming a plurality of charred hemp particles having more than 50% of particles formed between 1 and 2 microns in size comprising:
- drying cut hemp stalk on a field for a period of less than 7 days, said hemp stalk comprising hemp hurd and hemp fibers;
- pyrolyzing the dried hemp stalk at a temperature of greater than 1100° C. to create a char;
- adding the char to a grinding vessel and mechanically grinding the char for a period of between 1 and 16 hours by grinding, air jet milling, or ball milling the char to form a ground char having an irregular polyhedron shape;
- screening the ground char with a 2-micron screen to create a screened char of less than 2 microns;
- and
- capturing the screened char of less than 2 microns.
3 more elements
Dependencies are inferred from the claim text.