US 11,752,446 B2Granted

Plant and process for concentrating tartaric acid

AssigneeDistillerie Mazzari S.P.A

InventorEmidio Margheritini

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Abstract

A plant for concentrating a tartaric acid solution includes a first and a second evaporation unit arranged in series, a pump for feeding a diluted tartaric acid solution into the first evaporation unit, a barometric condenser placed downstream of the second evaporation unit, and a system for feeding a first low-temperature vapor into the first evaporation unit. A process for concentrating tartaric acid includes providing a plant according to the above description, performing a first concentration, by evaporation, of the diluted tartaric acid solution, inside the first evaporation unit, and performing a second concentration, by evaporation, of the partially concentrated tartaric acid solution from the first evaporation unit, inside the second evaporation unit. The plant and process for concentrating tartaric acid have the advantages of ensuring low energy consumption, allowing concentration of solutions tending to crystallization, and allowing the continuous measurement of the tartaric acid concentration to be concentrated.

A plant for concentrating a tartaric acid solution, the plant comprising:

a first evaporation unit and a second evaporation unit, wherein said first and second evaporation units are arranged in series;
a pump for feeding a diluted tartaric acid solution into said first evaporation unit;
a barometric condenser placed downstream of said second evaporation unit, and
a system for feeding a first low-temperature vapor into said first evaporation unit, wherein the first low-temperature vapor has a temperature comprised between 70° C. and 90° C.;
wherein each of said first and second evaporation units comprises:
(i) a heat-exchange evaporation chamber, in which vapor comes into contact with a tartaric acid solution to be concentrated,
(ii) a liquid-aeriform separation chamber, connected to a head portion of said heat-exchange evaporation chamber,
(iii) a connecting portion that connects the liquid-aeriform separation chamber to a bottom portion of said heat-exchange evaporation chamber, and
(iv) a recirculation pump for the tartaric acid solution, the recirculation pump operatively connected to said connecting portion;
and
wherein said first and second evaporation units are connected by a first pipe for transferring a partially concentrated tartaric acid solution, placed at a bottom portion of said first and second evaporation units, and by a second pipe for transferring a properly aeriform phase from a head portion of said liquid-aeriform separation chamber of said first evaporation unit to said heat-exchange evaporation chamber of said second evaporation unit,
wherein said connecting portion comprises a column that extends along a vertical axis, and
wherein said column of said connecting portion of said second evaporation unit comprises a pair of facing-flange pressure sensors spaced apart along the vertical axis of said column, each pressure sensor coupled to a tantalum fluid separator, and the pressure sensors configured to measure a difference in pressure along the vertical axis of said column.

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Abstract

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