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US 11,713,249 B2Granted
Continuous manufacture of graphenic compounds
AssigneesCornell University, Axium IP, LLC
InventorsYong Lak Joo, Mohammed Alamer, Brian Williams
Life of this patent
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Abstract
Provided herein are high throughput continuous or semi-continuous reactors and processes for manufacturing graphenic materials, such as graphene oxide. Such processes are suitable for manufacturing graphenic materials at rates that are up to hundreds of times faster than conventional techniques, have little batch-to-batch variation, have a high degree of tunability, and have excellent performance characteristics.
Claims12
A process for manufacturing a graphenic compound, the process comprising:
- a. injecting a first stock into a first inlet of a continuous or semi-continuous reactor, the first stock comprising graphite;
- b. optionally injecting a second stock into a second inlet of the continuous reactor or semi-continuous reactor, the second stock comprising potassium permanganate;
- c. optionally injecting a third stock into a third inlet of the continuous or semi-continuous reactor, the third stock comprising an oxidizing or quenching agent and being injected downstream from the injection point of the first and/or second stock(s);
- d. optionally injecting a fourth stock into a fourth inlet of the continuous reactor or semi-continuous reactor, the fourth stock comprising water and being injected downstream from the injection point of the first, second, and third stocks;
- and
- e. collecting the graphenic compound from an outlet of the continuous reactor or semi-continuous reactor, the graphenic compound being collected downstream from the injection points of the first, second, third, and fourth stocks,
- wherein the continuous reactor or semi-continuous reactor comprises a reactor chamber into which the first, second, third, and fourth stocks are injected;
- the reactor chamber being configured between an outer wall of a first cylindrical body and the inner wall of a second cylindrical body or bore, one or both of the first and/or second cylindrical bodies rotating around the axis thereof;
- and the first and second cylindrical bodies are rotating in opposite directions.
6 more elements
Dependencies are inferred from the claim text.