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US 11,684,901 B2Granted
Method for preparation of metal nanowires
AssigneeIntercomet, S.L.
InventorsMojtaba Meshkat Mamalek, Mohammad-Reza Azani, Azin Hassanpour, Nicoló Plaia
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Abstract
The present invention refers to a method for the preparation of zero-valent-transition metal nanowires such as crystalline silver nanowires, and to a reactor oven for the preparation of zero-valent-transition metal nanowires.
Claims13
A method for the preparation of zero-valent-transition metal nanowires comprising the steps of:
- i) providing a reaction mixture comprising:
- at least one capping agent, at least one transition metal salt, and at least one polar solvent;
- ii) adding the reaction mixture obtained in step (i) to at least one reactor;
- iii) heating the at least one reactor of step (ii) at a temperature between 30 and 300° C. for a period of time between 10 min and 7 days under a pressure of at least 100 KPa in a reactor oven to obtain a suspension comprising zero-valent-transition metal nanowires;
- wherein said at least one reactor comprises a longitudinal axis X-X′ and performs at least one of the following movements:
- a translational movement following a closed-path, and
- a rotational movement around the longitudinal axis X-X′ or around an axis W-W′ parallel to said longitudinal axis X-X′, at a constant frequency between 1 and 100 rpm;
- and
- iv) optionally performing a purification process of the suspension obtained in step (iii) to obtain a purified suspension comprising zero-valent-transition metal nanowires.
6 more elements
Dependencies are inferred from the claim text.