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US 11,661,677 B2Granted
Graphene fiber manufactured by joule heating and method of manufacturing the same
AssigneeIucf-Hyu (Industry-University Cooperation Foundation Hanyang University)
InventorsTae Hee Han, Sung Hyun Noh
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Abstract
A method of manufacturing a graphene fiber is provided. The method includes preparing a source solution including graphene oxide, supplying the source solution into a coagulation solution to form a graphene oxide fiber, reducing the graphene oxide fiber to form a primary graphene fiber, and Joule-heating the primary graphene fiber to form a secondary graphene fiber.
Claims15
A method of manufacturing a graphene fiber, the method comprising:
- preparing a source solution including graphene oxide;
- supplying the source solution from a spinneret into a coagulation solution to form a graphene oxide fiber;
- reducing the graphene oxide fiber to form a primary graphene fiber;
- and
- Joule-heating the primary graphene fiber to form a secondary graphene fiber,
- wherein the primary graphene fiber is Joule-heated such that amorphous carbon in the primary graphene fiber is crystallized,
- wherein, as a supply rate of the source solution supplied from the spinneret into the coagulation solution increases, a degree of orientation of a graphene sheet in the primary graphene fiber is high, a resistance of the primary graphene fiber is low, so that a value of a current applied to the primary graphene fiber for Joule-heating the primary graphene fiber increases in the Joule-heating of the primary graphene fiber to form the secondary graphene fiber.
4 more elements
A graphene fiber comprising:
- a secondary graphene fiber formed by Joule-heating a primary graphene fiber formed by reducing a graphene oxide fiber,
- wherein the secondary graphene fiber includes a plurality of graphene sheets agglomerated and extending in one direction,
- wherein a peak value of G-band of the secondary graphene fiber is greater than a peak value of D-band of the secondary graphene fiber, and
- wherein a grain size of the graphene sheets is 12.4 nm-34 nm, and a thickness of the graphene sheets is 5 nm-6.86 nm.
1 more element
Dependencies are inferred from the claim text.