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US 11,660,583 B2Granted
Treatment method for forming a dye sorbent
AssigneePrince Mohammad Bin Fahd University
InventorMuhammad Waqar Ashraf
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Abstract
A method for producing a modified sawdust sorbent. The method involves sulfonating sawdust with sulfuric acid and oxidizing the sulfonated sawdust with hydrogen peroxide. The method yields a modified sawdust sorbent containing sulfonated and oxidized cellulose. The modified sawdust sorbent has a higher surface area, higher organic dye adsorption capacity, and more rapid organic dye adsorption rate than unmodified sawdust. A method for organic dye removal from water includes using the modified sawdust sorbent to absorb dyes from water.
Claims9
Treatment method for forming a sorbent comprising:
- treating sawdust with sulfuric acid in a 4:3 weight ratio to form a sulfonating mixture,
- heating the sulfonating mixture at 100 to 200° C. to form a sulfonated sawdust,
- exposing the sulfonated sawdust to vacuum for at least 24 hours, then
- washing and drying the sulfonated sawdust at 50 to 150° C. to form a dried sawdust,
- treating the dried sawdust with a hydrogen peroxide solution to form a peroxide-treated sawdust,
- washing and drying the peroxide-treated sawdust at 50 to 150° C. to form a sulfonated and oxidized sawdust, and
- milling and sieving the sulfonated and oxidized sawdust to form the sorbent,
- wherein the sorbent has a dye adsorption capacity of 20 to 25 mg of dye per g of sorbent at 25 to 45° C.
5 more elements
Dependencies are inferred from the claim text.