Method for sulfonating sawdust to form modified sorbent
AssigneePrince Mohammad Bin Fahd University
InventorMuhammad Waqar Ashraf
Life of this patent
Estimating the term…
Abstract
A method for producing a modified sawdust sorbent. The method involves sulfonating sawdust with sulfuric acid and oxidizing the sulfonated sawdust with hydrogen peroxide. The method yields a modified sawdust sorbent containing sulfonated and oxidized cellulose. The modified sawdust sorbent has a higher surface area, higher organic dye adsorption capacity, and more rapid organic dye adsorption rate than unmodified sawdust. A method for organic dye removal from water includes using the modified sawdust sorbent to absorb dyes from water.
Claims11
A method of sulfonating sawdust to form a modified sawdust sorbent comprising:
- mixing the sawdust with sulfuric acid to form a sulfonating mixture,
- heating the sulfonating mixture at 100 to 200° C. to form a mixture comprising a liquid and a sulfonated sawdust,
- filtering and/or decanting the mixture to isolate the sulfonated sawdust,
- washing and drying the sulfonated sawdust at 50 to 150° C. to form a dried sawdust,
- treating the dried sawdust with a hydrogen peroxide solution to form a peroxide-treated sawdust,
- washing and drying the peroxide-treated sawdust at 50 to 150° C. to form a sulfonated and oxidized sawdust, and
- milling and sieving the sulfonated and oxidized sawdust to form the modified sawdust sorbent,
- wherein the modified sawdust sorbent has a dye adsorption capacity of 20 to 25 mg of dye per g of sorbent at 25 to 45° C.
Dependencies are inferred from the claim text.