Method for fabricating a hybrid carbon nanofiber product
AssigneeThe Florida International University Board of Trustees
InventorsArvind Agarwal, Ambreen Nisar, Lihua Lou, Benjamin Peter Boesl
Life of this patent
Estimating the term…
Abstract
Hybrid carbon nanofiber (Cnf) products (e.g., mats, yarns, webs, etc.) and methods of fabricating the same are provided. The hybrid Cnf products are flexible and lightweight and have high thermal conductivity. An electrospinning process can be used to fabricate the hybrid Cnf products and can include preparation of an electrospinning solution, electrospinning, and carbonization (e.g., under a vacuum condition).
Claims12
A method for fabricating a hybrid carbon nanofiber (Cnf) product decorated with particles, the method comprising:
- performing an electrospinning process on an electrospinning solution to give an intermediate product, the electrospinning solution comprising an organic compound and the particles;
- and
- performing a carbonization process on the intermediate product to give the Cnf product decorated with the particles,
- the carbonization process being performed under a vacuum condition,
- the carbonization process comprising:
- disposing the intermediate product on a surface of a predetermined shape;
- and
- performing an initial heating stage on the intermediate product on the surface at a first predetermined temperature for a first predetermined time, a plurality of intermediate heating stages on the intermediate product on the surface at respective predetermined temperatures for respective predetermined times, and a cooling stage on the intermediate product on the surface to cool the intermediate product from the predetermined temperature of a last stage of the plurality of intermediate heating stages to an ambient temperature, and the initial heating stage and the plurality of intermediate heating stages being preformed under the vacuum condition.
A method for fabricating a hybrid carbon nanofiber (Cnf) product decorated with particles, the method comprising:
- preparing an electrospinning solution by dissolving an organic polymer in a solvent to give a first intermediate solution, adding the particles to the first intermediate solution to give a second intermediate solution, and ultra-sonicating the second intermediate solution for a predetermined time to give the electrospinning solution;
- performing an electrospinning process on the electrospinning solution to give an intermediate product, the electrospinning solution comprising the organic polymer and the particles;
- and
- performing a carbonization process on the intermediate product to give the Cnf product decorated with the particles,
- the particles being hafnium carbide (HfC) nanoparticles,
- the carbonization process comprising:
- disposing the intermediate product on a surface of a predetermined shape;
- and
- performing an initial heating stage on the intermediate product on the surface at a first predetermined temperature for a first predetermined time, a plurality of intermediate heating stages on the intermediate product on the surface at respective predetermined temperatures for respective predetermined times, and a cooling stage on the intermediate product on the surface to cool the intermediate product from the predetermined temperature of a last stage of the plurality of intermediate heating stages to an ambient temperature,
- the initial heating stage and the plurality of intermediate heating stages being performed under a vacuum condition,
- the plurality of intermediate heating stages comprising at least four intermediate stages,
- the first predetermined temperature being in a range of from 200° C. to 250° C.,
- each respective predetermined temperature of the plurality of intermediate heating stages being in a range of from about 220° C. to about 800° C.,
- the predetermined temperature of the last stage of the plurality of intermediate heating stages being about 800° C.,
- the predetermined shape of the surface being a cuboid, and
- the hybrid Cnf product being a hybrid Cnf mat.
Dependencies are inferred from the claim text.