Method for producing an alumina gel having a high dispersibility and a specific crystallite size
AssigneeIfp Energies Nouvelles
InventorsMalika Boualleg, Olivier Lafon
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AssigneeIfp Energies Nouvelles
InventorsMalika Boualleg, Olivier Lafon
Estimating the term…
Process for preparing alumina gel in a single precipitation step consisting of dissolving an aluminium precursor, aluminium chloride, in water, at a temperature of 10° C. to 90° C. such that the pH of the solution is from 0.5 to 5, for a period of 2 to 60 minutes, then adjusting the pH to 7.5 to 9.5 by adding a basic precursor, sodium hydroxide, to the solution obtained to obtain a suspension, at a temperature of 5° C. to 35° C., and for 5 minutes to 5 hours, followed by a filtration step, said process not comprising any washing steps. Also, novel alumina gel having a high dispersibility index, in particular a dispersibility index of more than 80%, a crystallite dimension of 0.5 to 10 nm, a chlorine content of 0.001% to 2% by weight and a sodium content of 0.001% to 2% by weight, the percentages by weight being expressed with respect to the total weight of the alumina gel.
A process for the preparation of an alumina gel, wherein the alumina gel has a dispersibility index of more than 80%, a crystallite dimension, obtained by the Scherrer X ray diffraction formula along the crystallographic directions [020] and [120], respectively, in the range of 0.5 to 10 nm and in the range of 0.5 to 15 nm, a chlorine content in the range 0.001% to 2% by weight and a sodium content in the range 0.001% to 2% by weight, the percentages by weight being expressed with respect to the total weight of the alumina gel,
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