Method for the modification of wood
AssigneeTitan Wood Limited
InventorsBernardus Jozef Maria Pol, Stefan Van Dommele, Paul Bussemaker, Benjamin Painter, Gerrit Arie De Wit, Theodorus Gerardus Marinus Maria Kappen
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Abstract
The invention is directed to a process for the continuous acetylation of wood elements. The process particularly combines a batchwise impregnation step, with a continuous reaction step. In order to realize this, a collection step is built-in, so as to allow batches of impregnated wood elements to be fed into a reactor in a continuous manner. Very high acetylation contents can be obtained, at a level that had not been achievable before in a continuous and non-catalyzed acetylation process.
Claims17
A process for the acetylation of wood elements comprising the following steps:
- (a) impregnating a plurality of batches of wood elements with an acetylation fluid comprising acetic anhydride and/or acetic acid so as to provide a plurality of batches of impregnated wood elements comprising acetylation fluid comprising acetic anhydride and/or acetic acid, wherein the impregnating step is carried out in an impregnation chamber, wherein the impregnation chamber is configured to be closed off;
- (b) collecting, combining and storing said plurality of batches of impregnated wood elements comprising acetylation fluid comprising acetic anhydride and/or acetic acid in a collection chamber in such a manner as to provide a continuous feed of impregnated wood elements to a reaction chamber, the collection chamber is a vessel having an inlet, a place to collect and store a buffer volume of impregnated wood elements, an outlet for impregnated wood elements and a drain for separation of excess liquid from the wood elements, wherein said outlet for impregnated wood elements allows a controlled amount of impregnated wood elements to be fed into the reaction chamber, wherein the volume of the collection chamber is 1 to 15 times the volume of the impregnation chamber;
- (c) subjecting a continuous flow of impregnated wood elements to acetylation reaction conditions in said reaction chamber so as to provide a continuous flow of acetylated wood elements exiting said reaction chamber, wherein
- excess impregnation liquid is removed from the impregnated wood elements by transport of the impregnated wood elements through an upward tilted transport screw.
Dependencies are inferred from the claim text.