Method for preparing ZSM-5 zeolite
AssigneeKorea Research Institute of Chemical Technology
InventorsNa Young Kang, Yong Ki Park, Chang Hwan Kim, Yu Jin Lee
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Abstract
The present invention relates to a method for preparing ZSM-5 zeolite. The present invention can provide a method for preparing ZSM-5 zeolite comprising the steps of: preparing a first solution in a solution state by heating a mixture comprising a silica source, an alumina source, a neutralizing agent and a crystalline ZSM-5 nucleus; preparing a reaction mother liquid by mixing a second solution comprising salts into the first solution; and continuously crystallizing by continuously supplying the reaction mother liquid to a hydrothermal synthesis reactor, wherein formula [1] below is satisfied. 0.20≤Wa/Wb≤0.40 Formula [1]
Claims8
A method for preparing ZSM-5-based zeolite, the method comprising:
- heating a mixture including a silica source, an alumina source, a neutralizing agent, and a crystalline ZSM-5 nucleus to prepare a first solution in a solution state;
- mixing a second solution including a salt with the first solution to prepare a reaction mother liquor;
- and
- continuously supplying the reaction mother liquor to a hydrothermal synthesis reactor to perform continuous crystallization,
- wherein the following Equation 1 is satisfied:
- 0.2≤Wa/Wb≤0.40 [Equation 1]
- wherein Wa is a content of the salt in the reaction mother liquor, and Wb is a content of silica in the reaction mother liquor, and
- wherein the reaction mother liquor has a viscosity of 1000 to 2700 cP.
Dependencies are inferred from the claim text.