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US 11,478,772 B2Granted
Polymerisation unit and polymerisation process
AssigneeIneos Europe AG
InventorsErick Dominique Daire, Jean-Marc Galewski, Anthony Simoens, Arnaud Soulage
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Abstract
The present invention relates to processes and apparatus useful for (fast) ionic polymerisation of liquid monomer(s) containing reaction mixture for the production of the corresponding polymer(s).
Claims19
Polymerisation unit for ionic polymerisation of a liquid monomer(s) containing reaction mixture, comprising a polymerisation loop and a coolant loop and a heat exchanger reactor system (“HERS”) which is shared amongst the polymerisation loop and the coolant loop, wherein
- the polymerisation loop comprises a reaction mixture piping system connected to an inlet and an outlet of said HERS,
- the coolant loop comprises a coolant piping system connected to an inlet and an outlet of said HERS,
- the reaction mixture piping system comprises a circulating pump and the polymerisation loop comprises a polymer withdrawal system, characterised in that
- 1) the HERS comprises at least “x” parallel sections wherein a section shares its last coolant passage with the first coolant passage of the next section,
- 2) the said HERS' sections comprise “n” parallelepipedic channel(s) for the reaction mixture, “n” being an integer comprised between 2 and 20, and “n+1” passages for the coolant,
- 3) the flow paths of the reaction mixture in the “n” channel(s) of a section are unidirectionally parallel,
- 4) the flow paths of the coolant in the “n+1” passages of a section are unidirectionally parallel to the reaction mixture flow paths, and
- 5) the coolant is not in direct contact with the reaction mixture,
- 6) and wherein the dimensions of the reaction mixture parallelepipedic channels are characterised by
- a. a first dimension (“height”) comprised between 2 and 10 m,
- b. a second dimension (“depth”) comprised between 0.1 and 3 m, and
- c. a third dimension (“width”) comprised between 2 and 50 mm.
9 more elements
Dependencies are inferred from the claim text.