Microwave assisted and low-temperature fabrication of nanowire arrays on scalable 2D and 3D substrates
AssigneeUniversity of Connecticut
InventorsPu-Xian Gao, Xingxu Lu, Son Hoang
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Abstract
A method of making a titanium dioxide nanowire array includes contacting a substrate with a solvent comprising a titanium (III) precursor, an acid, and an oxidant while microwave heating the solvent, thereby forming a hydrogen titanate H2Ti2O5.H2O nanowire array. The hydrogen titanate nanowire array is annealed to form a titanium dioxide nanowire array. The substrate is seeded with titanium dioxide before starting the hydrothermal synthesis of the hydrogen titanate nanowire array. The titanium dioxide nanowire array is loaded with a platinum group metal to form an exhaust gas catalyst. The titanium dioxide nanowire array can be used to catalyze oxidation of combustion exhaust.
Claims35
A method of making a hydrogen titanate nanowire array, the method comprising:
- contacting a substrate with a solvent comprising a titanium (III) precursor, an acid, and an oxidant while microwave heating the solvent, thereby forming a hydrogen titanate nanowire array.
Dependencies are inferred from the claim text.