Process for the preparation of nanoparticles
AssigneesCentre National De La Recherche Scientifique, Institut National Polytechnique De Toulouse
InventorsMyrtil Kahn, Yohan Champouret, Richard Clergereaux, Constantin Vahlas, Anne-Francoise Mingotaud, Guillaume Carnide
Life of this patent
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Abstract
The present invention relates to a “safety-by-design” method for the preparation of nanoparticles, to a method for the preparation of a nanocomposite material, and to the use of a direct liquid injection device so as to prepare nanoparticles or nanocomposite materials in a “safety-by-design” process.
Claims19
A method for the preparation of nanoparticles selected from the group consisting of metal nanoparticles, metal oxide nanoparticles and semiconductor nanoparticles,
- wherein said method is implemented in a device comprising:
- at least one reacting chamber including at least one first inlet for admission of said liquid phase in said reacting chamber, at least one second inlet for admission of said gas phase in said reacting chamber, and an outlet for expulsion of said nanoparticles from said reacting chamber,
- a liquid injector arranged upstream of the first inlet for injecting or spraying said liquid phase into said reacting chamber,
- an injector of nanoparticles arranged downstream of the outlet for injecting or spraying said nanoparticles through an outlet of said nanoparticles injector, and
- control means for controlling the injection or the spray of said liquid phase and/or said nanoparticles, and wherein said method comprises:
- a step 1) of injecting a liquid phase comprising at least one nanoparticles precursor selected from the group consisting of precursors of metals, precursors of metal oxides and precursors of semiconductors in said reacting chamber through said liquid injector,
- a step 2) of contacting said liquid phase with a gas phase comprising at least one carrier gas and at least one reacting gas, said step 2) being carried out in said reacting chamber,
- a step 3) of reacting the nanoparticles precursor with the reacting gas so as to form nanoparticles, and
- a step 4) of expulsion of the nanoparticles produced in step 3) from the reacting chamber through the nanoparticles injector, said nanoparticles being under the form of an aerosol at the outlet of the nanoparticles injector.
A device comprising:
- at least one reacting chamber including at least one first inlet for admission of a liquid phase comprising at least one nanoparticles precursor selected from the group consisting of precursors of metals, precursors of metal oxides and precursors of semiconductors in said reacting chamber,
- at least one second inlet for admission of a gas phase comprising at least one carrier gas and at least one reacting gas in said reacting chamber, and
- an outlet for expulsion of nanoparticles selected from the group consisting of metal nanoparticles, metal oxide nanoparticles and semiconductor nanoparticles from said reacting chamber, wherein
- a liquid injector is arranged upstream of the first inlet for injecting or spraying said liquid phase into said reacting chamber,
- a nanoparticles injector is arranged downstream of the outlet for injecting or spraying said nanoparticles through an outlet of said nanoparticles injector, and
- a control means is configured to control the injection or the spray of said liquid phase and/or said nanoparticles, for the preparation of said nanoparticles or of a nanocomposite material, by contacting in the reacting chamber of the device the liquid phase comprising the at least one nanoparticles precursor with the gas phase comprising the at least one carrier gas and the at least one reacting gas.
Dependencies are inferred from the claim text.