# US 11,306,417 B2 · Bast-fiber material processing method

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- Number: US 11,306,417 B2
- Document ID: US11306417B2
- Status: Granted
- Kind: B2
- Application number: 15/502,802
- Filed: 2014-11-24
- Published: 2017-11-16
- Granted: 2022-04-19
- Earliest claimed: 2014-08-13
- Assignees: Syler Gibraltar Limited
- Applicants: Syler Gibraltar Limited
- Inventors: Vladimir Vladimirovich Maksimov
- Web page: https://patentgrep.com/patent/US11306417B2

## CPC

- D01G 21/00: Combinations of machines, apparatus, or processes, e.g. for continuous processing (D01G1/06, D01G9/12, D01G15/46, D01G15/94 take precedence)
- D01C 1/02: by chemical methods to obtain bast fibres
- D06M 10/00: Physical treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, e.g. by ultrasonic waves, corona discharge, irradiation, electric currents or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M 10/025: {Corona discharge or low temperature plasma}
- D06M 16/003: {with enzymes or microorganisms}
- D06M 2101/06: cellulosic
- D01G: PRELIMINARY TREATMENT OF FIBRES, e.g. FOR SPINNING (winding or unwinding, conducting or guiding laps, webs, slivers or rovings in general, sliver or roving cans, depositing in sliver or roving cabs B65H; preparation of fibres for paper-making D21)
- D01C: CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D06M: TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS

## Abstract

The invention relates to the textile industry, and specifically to methods for processing bast-fiber materials, for instance the fiber of flax, hemp, jute, nettle, kenaf, and others. The technical result which the present invention aims to achieve consists in: enhancing the quality of a cottonized fiber, when processing bast-fiber materials, by means of high-voltage electric pulse discharges following preliminary biochemical and final minimal mechanical processing; and in enhancing the physical/mechanical and spinning properties thereof, which, overall, allows for an optimized, efficient production process. Said technical result is achieved in that a bast-fiber material processing method includes a technological sequence of processes involving feeding raw material into a bale breaker, which is provided with a decompactor, and into a dosing system, processing using high-voltage electric pulse discharges, rinsing with emulsifying reagents, washing and press-drying in a drum-type installation, decompacting, final drying and light decompacting; the raw material is biochemically treated prior to being fed into high-voltage electric pulse discharge chambers.

## Claims

### Claim 1

A method of processing unscutched bast-fiber materials, comprising a woody part, cellulose, and encrusting substances, so as to elicit elementary fibers, comprising, in sequence, steps of:
a. feeding raw materials comprising intermediate products of bast-fiber materials after biological enzyme treatment without subsequent mechanical scutching into a bale-breaker with a loosener;
b. feeding the raw materials from said bale breaker with the loosener into a metering system;
c. biochemically treating the raw materials;
d. generating pulsed electric discharges between two electrodes disposed within a chamber containing a liquid medium and the biochemically treated raw materials so as to effectively generate enhanced hydraulic pressures and mechanical actions within the liquid medium, including shock waves and cavitation, which will tend to separate bast-fiber products from the raw materials, wherein said enhanced hydraulic pressures and mechanical actions result in generation of a discharge channel which expands at a rate of over 100 m/s and processing the biochemically treated raw materials in the chamber;
e. rinsing the bast-fiber products with emulsifying reagents; and
f. washing and pressing the bast-fiber products followed by loosening, final drying and fine loosening so as to obtain elementary fibers which retain the length, diameter and ordered crystalline structure of the cellulose in the bast-fiber material.

### Claim 2 (depends on 1)

The method according to claim 1, wherein the step of processing the biochemically treated raw material using a pulse electric discharge in a liquid medium causes separation of woody parts and encrusting substances from the elementary fibers.

### Claim 3 (depends on 1)

The method according to claim 1, wherein the liquid medium is water.

### Claim 4 (depends on 1)

The method according to claim 1, which further comprises a step of removing the used liquid medium using a filtration step prior to step (e).

### Claim 5 (depends on 1)

The method of claim 1, wherein the pulsed electric discharge has either (A) an energy of 2.2 kJ and is applied for 400 discharges; or (B) an energy of 3.6 kJ and is applied for between 100 and 200 discharges.

### Claim 6

A method of processing unscutched bast-fiber materials, comprising a woody part, cellulose, and encrusting substances, so as to elicit elementary fibers, comprising, in sequence, steps of:
a. feeding raw materials comprising intermediate products of bast-fiber materials after biological enzyme treatment without subsequent mechanical scutching into a bale-breaker with a loosener;
b. feeding the raw materials from said bale breaker with the loosener into a metering system;
c. biochemically treating the raw materials;
d. generating either (A) 400 pulsed electric discharges each having an energy of 2.2 kJ or (B) between 100 and 200 pulsed electric discharges each having an energy of 3.6 kJ, between two electrodes disposed within a chamber containing a liquid medium and the biochemically treated raw materials so as to effectively generate enhanced hydraulic pressures and mechanical actions within the liquid medium, including shock waves and cavitation, which will tend to separate bast-fiber products from the raw materials, and processing the biochemically treated raw materials in the chamber;
e. rinsing the bast-fiber products with emulsifying reagents; and
f. washing and pressing the bast-fiber products followed by loosening, final drying and fine loosening so as to obtain elementary fibers which retain the length, diameter and ordered crystalline structure of the cellulose in the bast-fiber material.

### Claim 7 (depends on 6)

The method according to claim 6, wherein the step of processing the biochemically treated raw material using a pulse electric discharge in a liquid medium causes separation of woody parts and encrusting substances from the elementary fibers.

### Claim 8 (depends on 6)

The method according to claim 6, wherein the liquid medium is water.

### Claim 9 (depends on 6)

The method according to claim 6, which further comprises a step of removing the used liquid medium using a filtration step prior to step (e).