# US 11,305,859 B2 · Method for forming a composite structure

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- Number: US 11,305,859 B2
- Document ID: US11305859B2
- Status: Granted
- Kind: B2
- Application number: 15/938,175
- Filed: 2018-03-28
- Published: 2019-10-03
- Granted: 2022-04-19
- Earliest claimed: 2018-03-28
- Assignees: The Boeing Company
- Applicants: The Boeing Company
- Inventors: Weidong Song; Gerard J. Gallo; Gwen Marie Lanphere Gross; Jamie J. Langabeer; Jason J. McBain; Stephen L. Metschan; Jeffrey H. Olberg; Max M. Osborne; Richard V. Phillips; Paul D. Evans; Hugh A. Yap; Nicholas J. Zayas
- Web page: https://patentgrep.com/patent/US11305859B2

## CPC

- B29C 70/865: {completely encapsulated}
- B29C 70/48: and impregnating the reinforcements in the closed mould, e.g. resin transfer moulding [RTM] {, e.g. by vacuum}
- B29C 70/542: {Placing or positioning the reinforcement in a covering or packaging element before or during moulding, e.g. drawing in a sleeve}
- B29C 70/86: Incorporated in coherent impregnated reinforcing layers, {e.g. by winding}
- B29D 99/0005: {Producing noodles, i.e. composite gap fillers, characterised by their construction}
- B64C 1/064: {Stringers; Longerons}
- B64C 1/12: Construction or attachment of skin panels
- B29L 2031/3076: {Aircrafts (blades, propellers B29L2031/08)}
- B64C 2001/0072: {from composite materials}
- Y02T 50/40: Weight reduction
- B29C: SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING (making preforms B29B11/00; making laminated products by combining previously unconnected layers which become one product whose layers will remain together B32B37/00 - B32B41/00)
- B29D: PRODUCING PARTICULAR ARTICLES FROM PLASTICS OR FROM SUBSTANCES IN A PLASTIC STATE (making granules B29B9/00; making preforms B29B11/00)
- B64C: AEROPLANES; HELICOPTERS
- B29L: INDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
- Y02T: CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO TRANSPORTATION

## Abstract

A method for forming a composite structure includes the steps of: forming a fiber-reinforced polymer paste to a shape of a cavity of a dry fiber preform structure; heating said dry fiber preform structure having said fiber-reinforced polymer in said cavity to an infusion temperature; infusing resin into said dry fiber preform structure and around said fiber-reinforced polymer; and curing said resin-infused fiber preform structure and said fiber-reinforced polymer at a cure temperature higher than said infusion temperature.

## Claims

### Claim 1

A method for forming a composite structure, comprising steps of:
providing a fiber-reinforced polymer paste to a cavity of a dry fiber preform structure, the fiber-reinforced polymer paste comprising resin and at least a first group of fibers dispersed within the resin;
heating the dry fiber preform structure having the fiber-reinforced polymer paste in the cavity to an infusion temperature; and
infusing resin into the dry fiber preform structure that has been heated and around the fiber-reinforced polymer paste that has been heated but not into the fiber-reinforced polymer paste that has been heated.

### Claim 2 (depends on 1)

The method of claim 1, further comprising compacting the fiber-reinforced polymer paste by applying pressure to form the fiber-reinforced polymer paste to a final shape using walls of the dry preform structure to help form the fiber-reinforced polymer paste to the final shape.

### Claim 3 (depends on 1)

The method of claim 1, wherein the at least a first gr of fibers dispersed within the resin include carbon nano-tubes.

### Claim 4 (depends on 1)

The method of claim 1, further comprising curing the fiber-reinforced poi paste and the infused resin at a cure temperature higher than said infusion temperature.

### Claim 5 (depends on 1)

The method of claim 1, wherein the step of providing the fiber-reinforced polymer paste to the cavity of the dry fiber preform structure includes extruding the fiber-reinforced polymer paste directly into the cavity.

### Claim 6 (depends on 1)

The method of claim 1, further comprising applying one or more additional dry fiber preforms after the fiber-reinforced polymer paste is provided to the cavity of the dry fiber preform structure and before the infusion of the resin.

### Claim 7 (depends on 1)

The method of claim 1, wherein the step of providing the fiber-reinforced polymer paste to the cavity of the dry fiber preform structure includes molding the fiber-reinforced polymer paste into the shape of the cavity and transferring the molded fiber-reinforced polymer to the cavity.

### Claim 8 (depends on 7)

The method of claim 7, further comprising partially curing the molded fiber-reinforced polymer paste before transferring the molded fiber-reinforced polymer paste to the cavity.

### Claim 9 (depends on 1)

The method of claim 1, further comprising preparing the fiber-reinforced polymer paste by mixing a group of fibers into a resin.

### Claim 10 (depends on 9)

The method of claim 9, wherein the prepared fiber-reinforced polymer paste is prepared as a batch of fiber-reinforced polymer paste, separated and provided to a plurality of cavities.

### Claim 11 (depends on 9)

The method of claim 9, wherein the step of mixing a group of fibers into said resin comprises:
adding a first group of fibers within the resin, the first group of fibers having a first length, wherein the first group of fibers has an aspect ratio of 2000 or less; and
adding a second group of fibers within the resin, the second group of fibers having a second length that is shorter than the first length.

### Claim 12 (depends on 11)

The method of claim 11, wherein the first group of fibers includes fibers having a length between 3 and 6 millimeters.

### Claim 13 (depends on 11)

The method of claim 11, wherein the first group of fibers comprises between 20% and 40% of a combined volume of the first and second groups of fibers; and the second group of fibers comprises between 60% and 80% by volume of the combined volume of the first and second group of fibers.

### Claim 14 (depends on 13)

The method of claim 13, wherein the combined volume of the first and second group of fibers comprises between 30% and 70% of a total volume of said fiber-reinforced polymer paste.

### Claim 15 (depends on 11)

The method of claim 11, further comprising adding a third group of fibers to the resin, the third group comprising carbon nano-tubes.

### Claim 16 (depends on 1)

The method of claim 1, further comprising adding thixotropic nanoparticles to the resin.

### Claim 17 (depends on 1)

The method of claim 1, further comprising adding a toughening agent to the resin.

### Claim 18 (depends on 1)

The method of claim 1, wherein the fiber-reinforced polymer paste comprises one or more of epoxy, phenolic, benzoxazine, and bis-maleimide (BMI) resins.

### Claim 19 (depends on 1)

The method of claim 1, wherein the fiber-reinforced polymer paste comprises one or more of carbon fibers and fiberglass.

### Claim 20 (depends on 1)

The method of claim 1, wherein the composite structure is an aircraft structural element.
