# US 11,299,839 B2 · Apparatus and method for treating a substrate with solid particles > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 11,299,839 B2 - Document ID: US11299839B2 - Status: Granted - Kind: B2 - Application number: 17/258,396 - Filed: 2019-07-12 - Published: 2021-09-23 - Granted: 2022-04-12 - Earliest claimed: 2018-07-13 - Assignees: Xeros Limited - Applicants: Xeros Limited - Inventors: Gareth Evan Lyn Jones; Christopher Holden; David Stevens - Web page: https://patentgrep.com/patent/US11299839B2 ## CPC - D06F 37/04: adapted for rotation or oscillation about a horizontal or inclined axis - D06F 35/006: {for washing or rinsing only} - D06F 37/06: Ribs, lifters, or rubbing means forming part of the receptacle - D06F 39/02: Devices for adding soap or other washing agents - D06F 37/02: Rotary receptacles, e.g. drums - D06F 37/065: {ribs or lifters having means for circulating the washing liquid} - D06F: LAUNDERING, DRYING, IRONING, PRESSING OR FOLDING TEXTILE ARTICLES ## Abstract Aspects relate to a drum (10) for rotatably mounting in an apparatus for use in the treatment of substrates with a solid particulate material; a method of treating a substrate comprising agitating the substrate in a drum (10); and a kit for converting an apparatus to comprise the drum (10). The drum has an inner surface (15) and an end wall (2) and access means (70) for introducing said substrates into said drum, wherein said drum (10) comprises: •(a) storage means (4) for storage of said solid particulate material, wherein at least part of said storage means is or comprises at least one cavity located in said end wall (2) of said drum (10); and•(c) a dispensing aperture (12) for dispensing solid particulate material from said storage means (4) into the interior of said drum (10), wherein said dispensing aperture (12) is comprised in said end wall (2) of said drum, characterised in that said drum (10) comprises a valve (6) that is actuatable between a closed position and an open position, wherein when said valve (6) is in said closed position said solid particulate material is prevented from passing through said dispensing aperture (12) and when said valve (6) is in said open position said solid particulate material is permitted to pass through said dispensing aperture (12). ## Claims ### Claim 1 A drum for rotatably mounting in an apparatus for use in the treatment of substrates with a solid particulate material, said drum having an inner surface and an end wall and access means for introducing said substrates into said drum, wherein said drum comprises: (a) storage means for storage of said solid particulate material, wherein at least part of said storage means is or comprises at least one cavity located in said end wall of said drum; and (c) a dispensing aperture for dispensing solid particulate material from said storage means into the interior of said drum, wherein said dispensing aperture is comprised in said end wall of said drum, characterised in that said drum comprises a valve that is actuatable between a closed position and an open position, wherein when said valve is in said closed position said solid particulate material is prevented from passing through said dispensing aperture and when said valve is in said open position said solid particulate material is permitted to pass through said dispensing aperture. ### Claim 2 (depends on 1) The drum according to claim 1, wherein said valve is actuatable between said closed position and said open position via a shaft. ### Claim 3 (depends on 2) The drum according to claim 2, wherein said shaft is substantially aligned with the rotational axis of said drum. ### Claim 4 (depends on 1) The drum according to claim 1, wherein said valve is manually actuatable. ### Claim 5 (depends on 1) The drum according to claim 1, wherein said valve is mechanically actuatable. ### Claim 6 (depends on 1) The drum according to claim 1, wherein said valve is electromechanically actuatable, in particular using a lead screw or a solenoid. ### Claim 7 (depends on 1) The drum according to claim 1, wherein said valve comprises a disk portion and a shank portion, and wherein when the valve is in the closed position, there is a gap between said disk portion of said valve and an edge of said dispensing aperture or said end wall of said drum, wherein the size of the gap is such that solid particulate material cannot pass through. ### Claim 8 (depends on 1) The drum according to claim 1, wherein said valve is or forms part of a poppet valve. ### Claim 9 (depends on 1) The drum according to claim 1, wherein said valve projects towards the interior of said drum when said valve is in the open position. ### Claim 10 (depends on 1) The drum according to claim 1, wherein said dispensing aperture is located substantially centrally in said end wall of said drum. ### Claim 11 (depends on 10) The drum of claim 10, wherein said dispensing aperture coincides with the rotational axis of said drum. ### Claim 12 (depends on 1) The drum of claim 1, wherein said drum comprises a plurality of said dispensing apertures. ### Claim 13 (depends on 12) The drum of claim 12, wherein the drum comprises a single valve. ### Claim 14 (depends on 12) The drum of claim 12, wherein the drum comprises a plurality of said valves, in particular the drum comprises a corresponding number of valves as dispensing apertures. ### Claim 15 (depends on 14) The drum of claim 14, wherein said plurality of valves are independently actuatable. ### Claim 16 (depends on 14) The drum of claim 14, wherein said plurality of valves are jointly actuatable, in particular by using an arrangement comprising an articulated rod. ### Claim 17 (depends on 1) The drum according to claim 1 wherein the storage means comprises multiple compartments, for instance, 2, 3, 4, 5 or 6 compartments, particularly wherein said multiple compartments are arranged so as to retain balance of the drum during rotation. ### Claim 18 (depends on 1) The drum according to claim 1, wherein the storage means comprises multiple compartments, wherein each of the compartments is defined by a cavity bound by a first wall and a second wall which each extend outwards from the rotational axis of the drum towards and preferably to the inner wall of the drum. ### Claim 19 (depends on 17) The drum according to claim 17, wherein each compartment is in fluid communication with its adjacent compartment or compartments such that solid particulate material, as well as any liquid medium, is able to pass from one compartment directly into an adjacent compartment during rotation of the drum by a communicating aperture in the wall between adjacent compartments, preferably wherein a communicating aperture exhibits a smallest dimension which is at least 4 times greater than the longest dimension of the solid particulate material, and preferably wherein the largest dimension of the communicating aperture is no greater than 50% of the longest dimension of a wall between adjacent compartments, and preferably wherein said communicating aperture is located in a wall between adjacent compartments at a point that is closer to the mid-point of said wall between adjacent compartments than to either the rotational axis of the drum or the inner wall of the drum. ### Claim 20 (depends on 17) The drum according to claim 17, wherein the multiple compartments are in fluid communication with a single dispensing aperture. ### Claim 21 (depends on 1) The drum according to claim 1, wherein the storage means further comprises one or more perforations which have dimensions smaller than the dimensions of the solid particulate material so as to permit passage of fluids through said perforations into and out of the storage means, particularly from or into the interior of said drum respectively, but to prevent egress of said solid particulate material through said perforations. ### Claim 22 (depends on 1) The drum according to claim 1, comprising a deflector for regulating the flow of solid particulate material through said dispensing aperture. ### Claim 23 (depends on 1) The drum according to claim 1, comprising a deflector configured to bias said solid particulate material within said storage means towards said dispensing aperture. ### Claim 24 (depends on 23) The drum according to claim 23, wherein said storage means comprises multiple compartments and each compartment comprises said deflector. ### Claim 25 (depends on 1) The drum according to claim 1, further comprising a guard positioned between the interior of said drum and said valve, wherein said guard comprises a plurality of apertures, wherein the plurality of apertures permit passage of solid particulate material through said guard but prevent passage of said substrates. ### Claim 26 (depends on 25) The drum according to claim 25, wherein said guard comprises a grill. ### Claim 27 (depends on 1) The drum according to claim 1, wherein said drum comprises a collecting means for facilitating flow of said solid particulate material from the interior of said drum to said storage means. ### Claim 28 (depends on 27) The drum according to claim 27, wherein said collecting means comprises at least one collecting aperture comprised in said end wall of said drum to facilitate flow of said solid particulate material from the interior of said drum to said storage means, wherein preferably said at least one collecting aperture is adjacent the periphery of the end wall of said drum. ### Claim 29 (depends on 27) The drum according to claim 27, wherein said collecting means comprises an elongate protrusion to facilitate flow of said solid particulate material from the interior of said drum to said storage means, wherein said elongate protrusion is located on said inner surface of said drum, wherein said elongate protrusion extends in a direction away from said end wall, wherein said elongate protrusion has an end proximal to the end wall and an end distal to the end wall. ### Claim 30 (depends on 29) The drum according to claim 29, wherein said elongate protrusion comprises a collecting aperture and a collecting flow path to facilitate flow of said particulate material from the interior of said drum to said storage means, wherein said collecting aperture in the elongate protrusion defines the start of said collecting flow path, and wherein said flow of said solid particulate material from the interior of the drum towards the storage means is facilitated by the rotation of said drum in a collecting direction. ### Claim 31 (depends on 29) The drum according to claim 29, wherein said elongate protrusion comprises: (a) a first collecting flow path to facilitate flow of said solid particulate material from the interior of said drum to a storage means in said drum when said drum rotates in a first collecting direction, and (b) a second collecting flow path to facilitate flow of said solid particulate material from the interior of said drum to said storage means when said drum rotates in a second collecting direction, wherein said second collecting direction is in the opposite rotational direction to said first collecting direction, and wherein said first collecting flow path and said second collecting flow path are different flow paths. ### Claim 32 (depends on 31) The drums according to claim 31, wherein said first flow path and said second flow path are symmetrically arranged along the length of said elongate protrusion. ### Claim 33 (depends on 29) The drum according to claim 29, wherein said drum comprises a plurality of said elongate protrusions. ### Claim 34 (depends on 33) The drum according to claim 33, wherein said drum comprises two, three, four, five or six of said elongate protrusions. ### Claim 35 (depends on 1) An apparatus for use in the treatment of substrates with a solid particulate material, said apparatus comprising a housing having mounted therein a rotatably mounted drum, wherein said drum is a defined in claim 1. ### Claim 36 (depends on 35) The apparatus according to preceding claim 35, which is configured such that for at least a part of said treatment said drum is tilted such that its axis defines an angle a to the horizontal plane which is greater than 0 and less than about 10° and such that said drum is inclined in a downwards direction from the front of said drum to the end wall of said drum. ### Claim 37 (depends on 35) The apparatus according to claim 35 wherein movement of said solid particulate material between the interior of the drum and the storage means is actuated entirely by rotation of the drum. ### Claim 38 (depends on 35) The apparatus according to claim 35, wherein the inner surface of said drum comprises perforations which have dimensions smaller than the dimensions of the solid particulate material so as to permit passage of fluids into and out of said drum but to prevent egress of said solid particulate material. ### Claim 39 (depends on 38) The apparatus according to claim 38, wherein said housing is a tub which surrounds said drum, preferably wherein said tub and said drum are substantially concentric, preferably wherein the walls of said tub are unperforated but having disposed therein one or more inlets and/or one or more outlets suitable for passage of a liquid medium and/or one or more treatment agents into and out of the tub. ### Claim 40 (depends on 35) The apparatus according to claim 35, wherein said drum has an opening at the opposite end of the drum to the end wall through which said substrates are introduced into said drum. ### Claim 41 (depends on 35) The apparatus according to claim 35, wherein the apparatus does not comprise a further storage means which is not attached to or integral with the drum, and/or wherein the apparatus does not comprise a pump for circulating said solid particulate material between the storage means and the interior of the drum. ### Claim 42 (depends on 35) The apparatus according to claim 35, which comprises said solid particulate material. ### Claim 43 (depends on 1) A method of treating a substrate, the method comprising agitating the substrate in a drum according to claim 1 with solid particulate material. ### Claim 44 (depends on 43) The method according to claim 43 wherein the solid particulate material is re-used in further treatment procedures according to the method. ### Claim 45 (depends on 43) The method according to claim 43 wherein the method is a method for treating multiple batches, wherein a batch comprises at least one substrate, the method comprising agitating a first batch with solid particulate material, wherein said method further comprises the steps of: (a) collecting said solid particulate material in the storage means; (b) agitating a second batch comprising at least one substrate with solid particulate material collected from step (a); and (c) optionally repeating steps (a) and (b) for subsequent batch(es) comprising at least one substrate. ### Claim 46 (depends on 43) The method according to claim 43, wherein the method for treating comprises a first period during which said valve is in said open position and a second period during which said valve is in said closed position. ### Claim 47 (depends on 46) The method of claim 46, wherein the duration of said first period is substantially equal to or exceeds the duration of said second period. ### Claim 48 (depends on 46) The method of claim 46, wherein said first period precedes said second period. ### Claim 49 (depends on 43) The method according to claim 43, wherein the method comprises agitating the substrate with solid particulate material and a liquid medium, preferably wherein the liquid medium is aqueous. ### Claim 50 (depends on 43) The method according to claim 43, wherein the method comprises agitating the substrate with said solid particulate material and a treatment formulation. ### Claim 51 (depends on 43) The method according to claim 43, wherein the substrate is or comprises a textile. ### Claim 52 (depends on 51) The method according to claim 51 wherein the treating of said substrate is cleaning, coloration, bleaching, abrading or ageing, or other textile or garment finishing process. ### Claim 53 (depends on 52) The method according to claim 52 for cleaning a substrate wherein the substrate is a soiled substrate. ### Claim 54 (depends on 35) A kit for converting an apparatus which is not suitable for use in the treatment of substrates using a solid particulate material into an apparatus according to claim 35 which is suitable for use in the treatment of substrates using a solid particulate material, wherein the apparatus comprises a housing having mounted therein a rotatably mounted drum having an inner surface and an end wall and which further comprises access means for introducing said substrates into said drum, and wherein said kit comprises: (a) solid particulate material; (b) storage means for storage of said solid particulate material, wherein at least part of said storage means is or comprises at least one cavity located in said end wall of said drum; (c) a dispensing aperture for dispensing solid particulate material from said storage means in to the interior of said drum, wherein said dispensing aperture is comprised in said end wall of said drum; and (d) a valve that is actuatable between a closed position and an open position, wherein when said valve is in said closed position said solid particulate material is prevented from passing through said dispensing aperture and when said valve is in said open position said solid particulate material is permitted to pass through said dispensing aperture. ### Claim 55 (depends on 35) A method of constructing an apparatus according to claim 35 which is suitable for use in the treatment of substrates using a solid particulate material, the method comprising retrofitting a starting apparatus which is not suitable for use in the treatment of substrates using a solid particulate material and which comprises a housing having mounted therein a rotatably mounted drum having an inner surface and an end wall and which further comprises access means for introducing said substrates into said drum, wherein said retrofitting comprises the steps of: (i) providing solid particulate material, providing one or more storage means for storage of solid particulate material, and providing one or more valves and, optionally, providing at least one elongate protrusion; (ii) affixing said storage means to one or more interior surface(s) of the drum, wherein at least part of said storage means is or comprises at least one cavity located in said end wall of said drum; (iii) providing a dispensing aperture for dispensing solid particulate material from said storage means into the interior of said drum in said end wall of said drum; (iv) affixing said valve to said end wall of said drum; and (v) optionally affixing to an interior surface of the drum said at least one elongate protrusion, wherein said valve is actuatable between a closed position and an open position, wherein when said valve is in said closed position said solid particulate material is prevented from passing through said dispensing aperture and when said valve is in said open position said solid particulate material is permitted to pass through said dispensing aperture.