Method for preparing inorganic halogenated lead cesium perovskite quantum dots and display device
AssigneeWuhan China Star Optoelectronics Semiconductor Display Technology Co., Ltd.
InventorXu Chen
Life of this patent
Estimating the term…
Abstract
A method for preparing inorganic halogenated lead perovskite quantum dots and a display device are provided. The method includes: a first coordination solution preparing step, a cesium oleate solution preparing step, a centrifugal separation step, a second coordination solution preparing step, a first ion exchange step, and a second ion exchange step. The present invention also provides a display device including a quantum dot layer, wherein luminescent quantum dots of the quantum dot layer are inorganic halogenated lead cesium perovskite quantum dots of the present invention.
Claims9
A method for preparing inorganic halogenated lead perovskite quantum dots (PQDs), comprising the following steps:
- a first coordination solution preparing step, comprising mixing and heating a first lead halide solid and a first solvent in a reaction vessel until the first lead halide solid is completely dissolved to obtain a first coordination solution;
- a cesium oleate solution preparing step, comprising mixing and heating a cesium carbonate solid and a second solvent in a container until the cesium carbonate solid is completely dissolved;
- a centrifugal separation step, comprising heating the first coordination solution and adding the cesium oleate solution to the first coordination solution, cooling the first coordination solution to room temperature to obtain a first mixed solution, and centrifuging the first mixed solution to obtain first quantum dots;
- a second coordination solution preparing step, comprising mixing and heating a second lead halide solid and the first solvent in a reaction vessel until the second lead halide solid is completely dissolved to obtain a second coordination solution;
- and
- a first ion exchange step, comprising re-dispersing the first quantum dots in a non-polar organic solvent, adding the second coordination solution dropwise to the non-polar organic solvent, performing an ion exchange reaction to obtain a second mixed solution, and centrifuging the second mixed solution to obtain second quantum dots;
- wherein
- the first quantum dots and the second quantum dots are both the inorganic halogenated lead perovskite quantum dots.
Dependencies are inferred from the claim text.