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US 11,219,652 B2Granted
Method for extracting herbal medicine
AssigneeShaanxi Panlong Pharmaceutical Group Limited By Share Ltd.
InventorsXiaolin Xie, Dezhu Zhang, Jianguo Meng, Yu Wang, Xuhua Zhou, Zhong Meng, Nan Hui, Juan Li
Life of this patent
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Abstract
A method for extracting herbal medicine includes: step one, spray extraction; step two, pressure filtration and concentration; step three, spray and countercurrent precipitation; and step four, concentrating reduced pressure and drying.
Claims3
A method for extracting an herbal medicine comprising:
- step one, spray extraction:
- pulverizing herbs to 100 to 120 mesh fine powder, adding the fine powder and an extracting solvent, in a ratio of 6-7 L extracting solvent/1 kg fine powder, to an agitation tank (1), stirring a mixture of the fine powder and extracting solvent at 80-100 r/min for 1-1.5 hours, spraying the mixture to an extraction tank (3) at a spraying speed of 400 to 600 L/h, adding first additional extracting solvent to fill two-thirds to three-fourths of the extraction tank (3), the mixture being sprayed 2-3 cm below a surface of the extracting solvent in the extraction tank (3), spraying countercurrently second additional extracting solvent from a bottom of the extraction tank (3) at a speed of 1000-1600 L/h to form an extraction solution, the second additional extracting solvent being pumped from an extracting solvent tank (6) at a pump pressure of 3.0-5.0 MPa, the step one, spray extraction being conducted at room temperature;
- step two, pressure filtration and concentration:
- discharging the extraction solution from step one to a filter press (4) to remove insoluble waste at a speed of 400-600 L/h and a pressure of 0.4-0.7 MPa to store at an extraction storage tank (5), pumping the extraction solution from the extraction storage tank (5) to a vacuum concentration tank (10), concentrating the extraction solution in the vacuum concentration tank (10) under 0.08 MPa to 0.1 MPa and at 60-80° C. to form a concentrated extraction solution with a solution density of 1.0-1.3, the extracting solvent being recycled to the extracting solvent tank (6);
- step three, spray and countercurrent precipitation:
- spraying the concentrated extraction solution to a tube centrifuge (12) at a speed of 200-400 L/h, adding a precipitation solvent to fill two-thirds to three-fourths of the tube centrifuge (12), the concentrated extraction solution being sprayed 2-3 cm below a surface of the precipitation solvent in the tube centrifuge (12), spraying countercurrently additional precipitation solvent from a bottom of the tube centrifuge (12) at a speed of 1000-1400 L/h and a pressure of 2.0-4.0 MPa to form a precipitation solution, centrifuging the precipitation solution and discharging a supernatant through an overflow outlet (20) of the tube centrifuge (12) to a resting tank (17) at a speed of 600-900 L/h, the supernatant being stored in the resting tank (17) for 24 hours;
- and
- step four, concentrating reduced pressure and drying:
- concentrating the supernatant from the resting tank (17) under reduced pressure, drying by vacuum spray and freeze-dry to obtain the herbal medicine.
6 more elements
Dependencies are inferred from the claim text.