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US 11,186,948 B2Granted
Method and a system for production of high molecular weight lignin
AssigneeFibratech Pte. Ltd
InventorMatti Kurki
Life of this patent
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Abstract
A cooking method and a digester system wherein partly digested cellulosic fiber source is compressed during cooking to provide high molecular weight lignin and pulp.
Claims8
A cooking method for production of high molecular weight lignin having a molecular weight of more than 2300 and pulp comprising:
- i. cooking a cellulosic fiber source comprising wood chips in a cooking liquor at a temperature selected from a range between 120° C. and 180° C. to a kappa number selected from a range between 100 and 5 to form a cooked cellulosic fiber source;
- ii. compressing the cooked cellulosic fiber source at the cooking temperature with a pressure selected from a range between 35 kPa and 1000 kPa, to provide a compressed cellulose fraction with a consistency higher than 10% by weight and a density selected from a range between 350 kg/m3 and 2000 kg/m3 in a black liquor comprising high molecular weight lignin comprising a molecular weight of more than 2300;
- iii. displacing the black liquor with a displacing liquor by pressing the compressed cellulose fraction in the black liquor with a pressure selected from a range between 1 kPa and 250 kPa to form a column having a consistency of at least 5% by weight, or a column porosity of at least 0.25, followed by displacing the black liquor with a displacing liquor having a lignin content lower than that in the black liquor, and wherein the pressure is lower than that in step ii;
- iv. recovering a high molecular weight lignin fraction having a molecular weight of more than 2300 from the displacing liquor;
- v. and recovering pulp from the compressed cellulose fraction.
2 more elements
Dependencies are inferred from the claim text.