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US 11,142,463 B2Granted
Method for producing silica aerogel blanket and silica aerogel blanket produced thereby
AssigneeLG Chem, Ltd.
InventorsMi Ri Kim, Je Kyun Lee, Kyoung Shil Oh
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Abstract
The present invention relates to a method for producing a silica aerogel blanket, the method comprising recovering a supercritical waste liquid generated after performing a step of supercritical drying, neutralizing the recovered supercritical waste liquid by adding an acid thereto for recycling, and reusing the recycled supercritical waste liquid, and a silica aerogel blanket produced thereby.
Claims7
A method for producing a silica aerogel blanket, comprising:
- producing a silica sol;
- preparing a wet gel-base material composite by immersing a base material for a blanket in the silica sol, and adding a base to perform gelation to yield the wet gel-base material composite;
- aging the wet gel-base material composite;
- surface modifying the aged wet gel-base material composite;
- supercritical drying the surface-modified wet gel-base material composite to produce the silica aerogel blanket and a supercritical waste liquid;
- recovering the supercritical waste liquid;
- neutralizing the recovered supercritical waste liquid by adding an acid thereto to yield a recycled supercritical waste liquid;
- and
- reusing the recycled supercritical waste liquid:
- (a) in producing the silica sol;
- or
- (b) in aging the wet gel-base material composite;
- or
- (c) in surface modifying the aged wet gel-base material composite;
- or
- (d) any combination of (a)-(c),
- wherein the acid is added in an amount of 0.2 to 1.5 parts by weight based on 100 parts by weight of the recovered supercritical waste liquid.
14 more elements
Dependencies are inferred from the claim text.