# US 11,028,336 B2 · Oil purification process

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- Number: US 11,028,336 B2
- Document ID: US11028336B2
- Status: Granted
- Kind: B2
- Application number: 16/337,726
- Filed: 2017-09-28
- Published: 2020-02-06
- Granted: 2021-06-08
- Earliest claimed: 2016-09-30
- Assignees: Neste Oyj
- Applicants: Neste Oyj
- Inventors: Annika Malm; Mervi Waddilove
- Web page: https://patentgrep.com/patent/US11028336B2

## CPC

- C11B 3/001: {by a combination of two or more of the means hereafter}
- C11B 3/006: {by extraction}
- C11B 3/008: {by filtration, e.g. including ultra filtration, dialysis (C11B3/005 takes precedence)}
- C11B 3/04: with acids
- C11B 3/10: by adsorption
- C11B 3/16: by mechanical means
- C11B: PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES (drying-oils C09F)

## Abstract

The invention relates to a process for purification of oil by heat treatment in order to degrade phospholipids present in the non-purified oil.

## Claims

### Claim 1

A method for purification of lipid material, the method comprising:
a) providing a feed of lipid material;
b) heat treating the lipid material without added water or other solvent wherein heat treatment takes place at any temperature in a range of 240° C. to 280° C., and wherein a residence time in step b) is maintained during a period of 1 minute to 30 minutes and wherein the lipid material has not undergone any pre-treatment prior to heating and wherein the heat treatment is performed in a pressure chamber; and
c) post treating the lipid material by a water treatment step which is performed in a presence of water in an amount of 1 wt % to 3 wt % to a volume of the lipid material;
wherein water treatment step c) is performed at a temperature of 130° C. to 220° C., to thereby reduce an amount of phosphorous and/or metal compounds in the lipid material.

### Claim 2 (depends on 1)

The method according to claim 1, wherein the lipid material is a plant based, microbial based or animal based lipid or any combination thereof.

### Claim 3 (depends on 1)

The method according to claim 1, comprising:
selecting a water content of the lipid material in the feed to be lower than 10000 ppm, lower than 5000 ppm, lower than 2000 ppm, lower than 1500 ppm, lower than 1000 ppm, lower than 500 ppm, lower than 250 ppm, lower than 100 ppm, lower than 50 ppm, lower than 25 ppm, lower than 10 ppm, lower than 5 ppm, lower than 1 ppm or such that the lipid feed is substantially water free.

### Claim 4 (depends on 1)

The method according to claim 1, comprising:
performing the water treatment step c) during a period of 1 minute to 30 minutes.

### Claim 5 (depends on 1)

The method according to claim 1, comprising:
removing water in the lipid material by evaporation.

### Claim 6 (depends on 1)

The method according to claim 1, comprising:
removing any impurities in the water treatment step c) by one or more of filtration, centrifugation or bleaching or any combinations thereof.

### Claim 7 (depends on 1)

The method according to claim 1, wherein post-treatment step c) comprises:
water washing/degumming or acid treatment/degumming or bleaching.

### Claim 8 (depends on 1)

The method according to claim 1, wherein post-treatment step c) comprises:
centrifugation and/or filtration to remove impurities formed during the process.

### Claim 9 (depends on 1)

The method according to claim 1, wherein post-treatment step c) comprises:
a bleaching treatment to remove impurities.

### Claim 10 (depends on 1)

The method according to claim 1, wherein phosphorous compounds are phospholipids, selected from one or more of phosphatidyl ethanolamines, phosphadityl cholines, phosphatidyl inositols or phosphatidic acids.

### Claim 11 (depends on 1)

A method for purification of lipid material according to claim 1, wherein a residence time in step b) is maintained during a period of 5 minutes to 30 minutes.

### Claim 12

The method according to 1, comprising:
performing the water treatment step c) during a period of 5 minutes to 30 minutes.