Method for treating an elastomer packaging element, and packaging element thus treated
AssigneeAptar Stelmi SAS
InventorsLaurent Caburet, Ghislain Fournier
Life of this patent
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Abstract
A method of treating an elastomer packaging element (10), in particular a stopper for medical or pharmaceutical use, the packaging element (10) having a bottom portion (11) that is to penetrate into a neck (21) of a container (20) and a top portion (12) that is to co-operate in sealed manner with a top surface (22) of said neck (21) of the container (20). The top surface of the top portion (12) is treated by a plasma-assisted polymerization method at atmospheric pressure using a plasma flame created at atmospheric pressure and into which a monomer is injected, the monomer polymerizing on the top surface in order to form a coating (18).
Claims8
A method of treating an elastomer packaging element, said packaging element having a bottom portion configured to penetrate into a neck of a container and a top portion configured to remain external to the container and having a top surface, the packaging element is configured to co-operate with a distal end surface of said neck of the container so as to seal the container, said method comprising a stage of atmospheric plasma- assisted surface activation of the top surface and a subsequent stage of atmospheric plasma- assisted deposition on the top surface,
- wherein said atmospheric plasma-assisted surface activation stage comprises, at atmospheric pressure, passing a first plasma flame over said top surface, wherein:
- a gas used for generating the first plasma flame is nitrogen,
- a speed at which the first plasma flame passes over said top surface is 100 mm/s to 500 mm/s,
- a number of passes over said top surface to perform the activation is one cycle,
- a flow rate of the gas for generating the first plasma flame is 10 L/min to 100 L/min, and
- a distance between the nozzle where the first plasma flame is generated and said top surface is in the range of 5 mm to 35 mm, and
- wherein said atmospheric plasma-assisted deposition stage comprises passing, at atmospheric pressure, a second plasma flame over said top surface, wherein:
- a gas used for generating the second plasma flame is air,
- a speed at which the second plasma flame passes over said top surface is 100 mm/s to 500 mm/s,
- a number of passes over said top surface to perform the deposition is two cycles,
- a gas flow rate of the gas for generating the second plasma flame is 10 L/min to 100 L/min,
- a distance between the nozzle where the second plasma flame is generated and said top surface is in the range of 5 mm to 35 mm;
- and
- a monomer is injected into said second plasma flame, said monomer polymerizing on the top surface to form a coating.
Dependencies are inferred from the claim text.