Ripening of 1,4-bis (4-phenoxybenzoyl)benzene
AssigneeArkema France
InventorsJulien Jouanneau, Jérôme Amstutz, Guillaume Vincent
Life of this patent
Estimating the term…
Loading patent…
AssigneeArkema France
InventorsJulien Jouanneau, Jérôme Amstutz, Guillaume Vincent
Estimating the term…
A method for manufacturing 1,4-bis(4-phenoxybenzoyl)benzene, including: reacting terephthaloyl chloride with diphenyl ether in a reaction solvent and in the presence of a Lewis acid, so as to obtain a product mixture including a 1,4-bis(4-phenoxybenzoyl)benzene-Lewis acid complex; contacting the product mixture with a protic solvent, so as to obtain a first phase containing the Lewis acid and a second phase containing 1,4-bis(4-phenoxybenzoyl)benzene; heating at least the second phase up to a maximum temperature, followed by cooling the second phase down to a separation temperature; subjecting at least the second phase to a solid/liquid separation step at the separation temperature, so as to recover solid 1,4-bis(4-phenoxybenzoyl)benzene.
A method for manufacturing 1,4-bis(4-phenoxybenzoyl)benzene, comprising:
Dependencies are inferred from the claim text.