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US 10,894,844 B2Granted
Superabsorbent polymer and preparation method thereof
AssigneeLG Chem, Ltd.
InventorsYong Hun Lee, Tae Young Won, Jun Wye Lee, Kwangin Shin, Chang Hun Han
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Abstract
Provided are a superabsorbent polymer having a high bulk density value and showing a reduction in unpleasant odors which may be caused by various additives included in a preparation process while basically maintaining excellent absorption performance and absorption rate, and a preparation method thereof.
Claims9
A method of preparing a superabsorbent polymer, the method comprising:
- A) performing crosslinking polymerization of water-soluble ethylene-based unsaturated monomers having acidic groups which are at least partially neutralized, in the presence of an internal crosslinking agent, to form a water-containing gel polymer including a crosslinked polymer;
- B) drying, pulverizing, and size-sorting the water-containing gel polymer to form a base polymer powder;
- C) performing surface-crosslinking of the base polymer powder by heat treatment in the presence of a surface crosslinking agent to form superabsorbent polymer particles;
- D) adding an aggregation inhibitor and water to the superabsorbent polymer particles;
- and
- E) evaporating the water,
- wherein an aging process is performed at a temperature of 50° C. to 120° C. and a pressure of 100 mm H2O to less than 1500 mm H2O for 5 minutes to 2 hours, after adding water and the aggregation inhibitor.
4 more elements
Dependencies are inferred from the claim text.