# US 10,872,827 B2 · Manufacturing method and evaluation method for SiC device

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- Number: US 10,872,827 B2
- Document ID: US10872827B2
- Status: Granted
- Kind: B2
- Application number: 16/514,114
- Filed: 2019-07-17
- Published: 2020-01-23
- Granted: 2020-12-22
- Earliest claimed: 2018-07-19
- Assignees: Showa Denko K.K.
- Applicants: Showa Denko K.K.
- Inventors: Ling Guo
- Web page: https://patentgrep.com/patent/US10872827B2

## CPC

- H10P 74/203: {Structural properties, e.g. testing or measuring thicknesses, line widths, warpage, bond strengths or physical defects}
- G01N 21/6489: {Photoluminescence of semiconductors}
- G01N 21/9501: {Semiconductor wafers (manufacturing processes per se of semiconductor devices implementing a measuring step H10P74/20)}
- G01N 27/00: Investigating or analysing materials by the use of electric, electrochemical, or magnetic means (G01N3/00 – G01N25/00 take precedence; measurement or testing of electric or magnetic variables or of electric or magnetic properties of materials G01R)
- H10P 30/28: characterised by an annealing step, e.g. for activation of dopants
- H10P 74/207: {Electrical properties, e.g. testing or measuring of resistance, deep levels or capacitance-voltage characteristics}
- H10P 74/23: {characterised by multiple measurements, corrections, marking or sorting processes}
- G01N 2021/8427: {Coatings}
- H10P 30/2042: {into crystalline silicon carbide}
- H10P 30/21: {of electrically active species}
- H10P: GENERIC PROCESSES OR APPARATUS FOR THE MANUFACTURE OR TREATMENT OF DEVICES COVERED BY CLASS H10
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)

## Abstract

Provided is a manufacturing method for a SiC device including: performing an ion implantation process of implanting ions in an epitaxial layer of a SiC epitaxial wafer that has the epitaxial layer; and performing an evaluation process of evaluating a defect of the SiC epitaxial wafer after the ion implantation process, in which the evaluation process includes a surface inspection process of inspecting a surface of the SiC epitaxial wafer, a PL inspection process of irradiating a region that includes the defect detected in the surface inspection to perform photoluminescence measurement after the surface inspection process, and a determination process of determining a degree of the defect from a surface defect image detected in the surface inspection and a PL defect image detected in the PL inspection process.

## Claims

### Claim 1

A manufacturing method for a SiC device, comprising:
performing an ion implantation process of implanting ions in an epitaxial layer of a SiC epitaxial wafer that has the epitaxial layer; and
performing an evaluation process of evaluating a defect of the SiC epitaxial wafer after the ion implantation process,
wherein the evaluation process includes
a surface inspection process of inspecting a surface of the SiC epitaxial wafer,
a photoluminescence inspection process of irradiating a region that includes the defect detected in the surface inspection with excitation light to perform photoluminescence measurement after the surface inspection process, and
a determination process of determining a degree of the defect from a surface defect image detected in the surface inspection and a photoluminescence defect image detected in the photoluminescence inspection process,
wherein in the photoluminescence inspection process, the defect evaluated in the evaluation process is determined as being defective in a case in which a ratio between luminance S at a light emitting portion that emits light and light emitting intensity N at a light non-emitting portion that does not emit light is equal to or greater than 4.0.

### Claim 2 (depends on 1)

The manufacturing method for a SiC device according to claim 1, further comprising:
performing an electric strength measurement process of applying a voltage to each produced SiC device to perform electric strength measurement after the evaluation process.

### Claim 3 (depends on 2)

The manufacturing method for a SiC device according to claim 2, wherein in the photoluminescence inspection process, the defect evaluated in the evaluation process is determined as being defective in a case in which the ratio between the luminance S at the light emitting portion that emits light and light emission intensity N at the light non-emitting portion that does not emit light is equal to or greater than 2.0.

### Claim 4 (depends on 1)

The manufacturing method for a SiC device according to claim 1, wherein in the photoluminescence inspection process, the defect evaluated in the evaluation process is determined as being defective in a case in which the ratio between the luminance S at the light emitting portion that emits light and light emission intensity N at the light non-emitting portion that does not emit light is equal to or greater than 2.0.

### Claim 5

An evaluation method for a SiC device, comprising:
performing a surface inspection process of inspecting a surface of a SiC epitaxial wafer;
performing a photoluminescence inspection process of irradiating the surface of the SiC epitaxial wafer with excitation light to perform photoluminescence measurement; and
performing a determination process of determining a degree of defect from a surface defect image detected in the surface inspection and a photoluminescence defect image detected in the PL inspection process,
wherein in the photoluminescence inspection process, the defect evaluated in the evaluation process is determined as being defective in a case in which a ratio between luminance S at a light emitting portion that emits light and light emitting intensity N at a light non-emitting portion that does not emit light is equal to or greater than 4.0.

### Claim 6 (depends on 5)

The evaluation method for a SiC device as claimed in claim 5,
wherein in the photoluminescence inspection process, the defect evaluated in the evaluation process is determined as being defective in a case in which the ratio between the luminance S at the light emitting portion that emits light and light emission intensity N at the light non-emitting portion that does not emit light is equal to or greater than 2.0.
