# US 10,870,148 B2 · Aluminum alloy powder metal with transition elements

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- Number: US 10,870,148 B2
- Document ID: US10870148B2
- Status: Granted
- Kind: B2
- Application number: 13/993,942
- Filed: 2011-12-14
- Published: 2013-11-21
- Granted: 2020-12-22
- Earliest claimed: 2010-12-15
- Assignees: GKN Sinter Metals, LLC
- Applicants: Donald Paul Bishop; Richard L. Hexemer, Jr.; Ian W. Donaldson; Randy William Cooke
- Inventors: Donald Paul Bishop; Richard L. Hexemer, Jr.; Ian W. Donaldson; Randy William Cooke
- Web page: https://patentgrep.com/patent/US10870148B2

## CPC

- B22F 9/082: {atomising using a fluid (using centrifugal force B22F9/10)}
- B22F 1/12: Metallic powder containing non-metallic particles (containing lubricating or binding agents or organic material B22F1/10)
- C22C 32/0047: {with carbides, nitrides, borides or silicides as the main non-metallic constituents}
- B22F 2998/10: Processes characterised by the sequence of their steps
- B22F: WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER (making alloys by powder metallurgy C22C); APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- C22C: ALLOYS (treatment of alloys C21D, C22F)

## Abstract

A transition element-doped aluminum powder metal and a method of making this powder metal are disclosed. The method of making includes forming an aluminum-transition element melt in which a transition element content of the aluminum-transition element melt is less than 6 percent by weight. The aluminum-transition element melt then powderized to form a transition element-doped aluminum powder metal. The powderization may occur by, for example, air atomization.

## Claims

### Claim 1

A method of making a powder metal part, the method comprising:
forming an aluminum-transition element melt consisting of a 2324 aluminum alloy with additions of transition elements of 1 weight percent iron and 1 weight percent nickel as a total weight percent of the aluminum-transition element melt;
powderizing the aluminum-transition element melt to form a transition element-doped aluminum powder metal; and
compacting and sintering the transition element-doped aluminum powder metal to form the powder metal part in which compacting and sintering the transition element-doped aluminum powder metal to form the powder metal part involves separately compacting the transition element-doped aluminum powder metal to form a compact and then subsequently sintering the compact, wherein the sintering consists of heating in a furnace environment to form the powder metal part;
wherein a concentration of the transition elements in the powder metal part is equal to a concentration of the transition elements found in the transition element-doped aluminum powder metal used to form the powder metal part and wherein the concentration of the transition elements in the powder metal part is equal to a concentration of the transition elements found in the aluminum-transition element melt.

### Claim 2 (depends on 1)

The method of claim 1, wherein the step of powderizing includes air atomizing the aluminum-transition element melt.

### Claim 3 (depends on 1)

The method of claim 1, wherein powderizing the aluminum-transition element melt to form a transition element-doped aluminum powder metal includes at least one of atomizing with a gas, comminution, grinding, chemical reaction, and electrolytic deposition.

### Claim 4 (depends on 3)

The method of claim 3, wherein the gas is one of argon, nitrogen, and helium.

### Claim 5 (depends on 1)

The method of claim 1, wherein the powder metal part formed from the transition element-doped aluminum powder metal has fewer intermetallics formed along grain boundaries of the part in comparison to a powder metal part made from a powder metal of similar composition but with the transition element added as an elemental powder or as part of a master alloy.

### Claim 6

A method of making a powder metal part, the method comprising:
forming an aluminum-transition element melt consisting of a 2324 aluminum alloy with additions of transition elements of 1 weight percent iron and 1 weight percent nickel as a total weight percent of the aluminum-transition element melt;
powderizing the aluminum-transition element melt to form a transition element-doped aluminum powder metal in which a concentration of the transition elements in the transition element-doped aluminum powder metal is equal to a concentration of the transition elements found in the aluminum-transition element melt; and
compacting and sintering a mixture consisting of the transition element-doped aluminum powder metal and at least one ceramic additive up to 15 volume percent to form the powder metal part in which compacting and sintering the transition element-doped aluminum powder metal and the at least one ceramic additive to form the powder metal part involves compacting the transition element-doped aluminum powder metal and the at least one ceramic additive to form a compact and then subsequently sintering the compact, wherein the sintering consists of heating in a furnace environment to form the powder metal part.

### Claim 7

A method of making a powder metal part, the method comprising:
forming an aluminum-alloying element melt consisting of a 2324 aluminum alloy with additions of alloying elements of 1 weight percent iron and 1 weight percent nickel as a total weight percent of the aluminum-alloying element melt;
powderizing the aluminum-alloying element melt to form an alloying element-doped aluminum powder metal wherein the alloying elements form an intermetallic phase with the aluminum and wherein the intermetallic phase is homogenously dispersed throughout alloying element-doped aluminum powder metal; and
compacting and sintering the alloying element-doped aluminum powder metal to form the powder metal part in which compacting and sintering the alloying element-doped aluminum powder metal to form the powder metal part involves separately compacting the alloying element-doped aluminum powder metal to form a compact and then subsequently sintering the compact, wherein the sintering consists of heating in a furnace environment to form the powder metal part;
wherein a concentration of the alloying elements in the powder metal part is equal to a concentration of the alloying elements found in the alloying element-doped aluminum powder metal used to form the powder metal part and wherein the concentration of the alloying elements in the powder metal part is equal to a concentration of the alloying elements found in the aluminum-alloying element melt.

### Claim 8 (depends on 6)

The method of claim 6, wherein at least one ceramic additive is SiC.

### Claim 9 (depends on 6)

The method of claim 6, wherein at least one ceramic additive is AIN.
