# US 10,870,091 B2 · System for dissolving solid chemicals and generating liquid solutions > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 10,870,091 B2 - Document ID: US10870091B2 - Status: Granted - Kind: B2 - Application number: 16/274,789 - Filed: 2019-02-13 - Published: 2019-08-15 - Granted: 2020-12-22 - Earliest claimed: 2018-02-13 - Assignees: Ecolab USA Inc. - Applicants: Ecolab USA Inc. - Inventors: Kenneth Thomas Dobizl; Amit Gupta; Alessandro Culotti; Joshua James Lanz; Trishul Artham - Web page: https://patentgrep.com/patent/US10870091B2 ## CPC - B01F 21/30: {Workflow diagrams or layout of plants, e.g. flow charts; Details of workflow diagrams or layout of plants, e.g. controlling means} - B01F 21/221: {comprising constructions for blocking or redispersing undissolved solids} - B01F 25/50: Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle - B01F 35/2112: {Level of material in a container or the position or shape of the upper surface of the material} - B01F 35/2132: {Concentration, pH, pOH, p(ION) or oxygen-demand (B01F35/2133 takes precedence)} - B01F 35/2209: {Controlling the mixing process as a whole, i.e. involving a complete monitoring and controlling of the mixing process during the whole mixing cycle} - B01F 35/2211: {Amount of delivered fluid during a period} - B01J 4/008: {Feed or outlet control devices} - B01F 21/40: {characterised by the state of the material being dissolved} - B01F 21/503: {Filters} - B01F: MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING (mixing paints B44D3/06) - B01J: CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS ## Abstract A system for dissolving solid chemical may include three reservoirs positioned in a vertically stacked arrangement. A solid chemical reservoir configured to receive solid chemical to be dissolved may be nested in a solution generator reservoir into which water is introduced to erode the solid chemical. A dissolved chemical reservoir can be positioned under the solid chemical reservoir and the solution generator reservoir. The dissolved chemical reservoir can store solution generated using the system. In some examples, a recirculation circuit is used to recirculate water introduced into the solution generator reservoir until a solution having a target concentration of the chemical being dissolved is achieved. The recirculation circuit may include a recirculation line having an outlet aimed at the bottom wall of the solid chemical reservoir. ## Claims ### Claim 1 A system for dissolving solid chemical comprising: a solid chemical reservoir configured to receive solid chemical to be dissolved, the solid chemical reservoir have a porous bottom wall and at least one sidewall extending vertically upwardly from the porous bottom wall; a solution generator reservoir surrounding the porous bottom wall and at least a portion of the sidewall of the solid chemical reservoir, the solution generator reservoir having an opening through which dissolved chemical generated in the solution generator reservoir is configured to be discharged; a dissolved chemical reservoir in selective fluid communication with the solution generator reservoir via the outlet opening; a recirculation circuit that includes a recirculation pump and a recirculation line having an outlet aimed at the porous bottom wall, the pump being configured to draw fluid from the solution generator reservoir and discharge the fluid through the outlet of the recirculation line; and a controller configured to: control addition of water to the solution generator reservoir at least until the porous bottom wall of the solid chemical reservoir is submerged in the water; control the recirculation circuit to recirculate fluid in the solution generator reservoir to generate a solution having a target concentration of the solid chemical via erosion of solid chemical in the solid chemical reservoir; and control discharge of the solution to the dissolved chemical reservoir. ### Claim 2 (depends on 1) The system of claim 1, further comprising a delivery pump configured to draw solution from the dissolved chemical reservoir and deliver pressurized solution, wherein the delivery pump is configured to operate at a higher pressure and lower volume than the recirculation pump. ### Claim 3 (depends on 1) The system of claim 1, further comprising a generator housing in which the solid chemical reservoir, the solution generator reservoir, the dissolved chemical reservoir, and the recirculation circuit are provided, wherein the solid chemical reservoir and the solution generator reservoir are positioned over a top surface of the solution generator reservoir. ### Claim 4 (depends on 3) The system of claim 3, wherein the solution generator reservoir has a bottom wall and at least one sidewall defining a cavity into which the solid chemical reservoir is inserted, and the sidewall of the solution generator reservoir is offset from the generator housing to define a space in which the recirculation pump is positioned. ### Claim 5 (depends on 3) The system of claim 3, further comprising a chemical dispensing docking station positioned on a top surface of the generator housing over the solid chemical reservoir. ### Claim 6 (depends on 1) The system of claim 1, wherein the outlet of the recirculation line is positioned under the sidewall of the solid chemical reservoir. ### Claim 7 (depends on 1) The system of claim 1, wherein the outlet of the recirculation line is positioned co-planar with the porous bottom wall of the solid chemical reservoir. ### Claim 8 (depends on 1) The system of claim 1, wherein the porous bottom wall has a conical shape. ### Claim 9 (depends on 1) The system of claim 1, further comprising at least one filter layer secured to the porous bottom wall of the solid chemical reservoir. ### Claim 10 (depends on 1) The system of claim 1, wherein the opening of the solution generator reservoir is in selective fluid communication to a water line via a valve and the controller is configured to control addition of water through the opening by controlling the valve. ### Claim 11 (depends on 1) The system of claim 1, further comprising a sensor configured to generate information indicative of the concentration of the solid chemical in the fluid, wherein the controller is configured to control the recirculation circuit to terminate recirculation of fluid in the solution generator reservoir when information received from the sensor indicates that the fluid has reached the target concentration. ### Claim 12 (depends on 1) The system of claim 1, wherein the controller is configured to discharge solution in the dissolved chemical reservoir after the solution has been in the dissolved chemical reservoir a threshold amount of time and generate a fresh batch of the solution. ### Claim 13 A method comprising: introducing water into a solution generator reservoir that surrounds a porous bottom wall and at least a portion of a sidewall of a solid chemical reservoir containing solid chemical to be dissolved until a height of water in the solution generator reservoir wets some but not all of the solid chemical in the solid chemical reservoir; recirculating fluid in the solution generator reservoir by drawing fluid out of the solution generator reservoir with a pump and reintroducing the fluid into the solution generator reservoir through a recirculation line having an outlet aimed at the porous bottom wall of the solid chemical reservoir, wherein fluid is recirculated until a solution having a target concentration is generated via dissolution of solid chemical in the solid chemical reservoir; discharging the solution from the solution generator reservoir into a dissolved chemical reservoir. ### Claim 14 (depends on 13) The method of claim 13, further comprising drawing solution from the dissolved chemical reservoir with a delivery pump and delivering pressurized solution, wherein the delivery pump operates at a higher pressure and lower volume than the pump used to recirculate fluid. ### Claim 15 (depends on 13) The method of claim 13, further comprising a generator housing in which the solid chemical reservoir, the solution generator reservoir, the dissolved chemical reservoir, and the pump are provided, wherein the solid chemical reservoir and the solution generator reservoir are positioned over a top surface of the solution generator reservoir and discharging the solution from the solution generator reservoir into the dissolved chemical reservoir comprises conveying the solution vertically downwards from the solution generator reservoir into the dissolved chemical reservoir within the generator housing. ### Claim 16 (depends on 15) The method of claim 15, further comprising engaging a reservoir containing chemical to be added to the solid chemical reservoir with a chemical dispensing docking station positioned on a top surface of the generator housing, and opening the reservoir to add the solid chemical to the solid chemical reservoir. ### Claim 17 (depends on 13) The method of claim 13, wherein the outlet of the recirculation line is positioned under the sidewall of the solid chemical reservoir. ### Claim 18 (depends on 13) The method of claim 13, wherein the outlet of the recirculation line is positioned co-planar with the porous bottom wall of the solid chemical reservoir. ### Claim 19 (depends on 13) The method of claim 13, further comprising measuring information indicative of the concentration of the solid chemical in the fluid, and terminating recirculation of the fluid based on received information indicating that the fluid has reached the target concentration. ### Claim 20 (depends on 13) The method of claim 13, wherein introducing water into the solution generator reservoir comprises introducing water through an opening in the solution generator reservoir, and discharging the solution from the solution generator reservoir into the dissolved chemical reservoir comprises discharging the solution through the same opening in the solution generator reservoir through which water was introduced.