# US 10,865,524 B2 · Paper composition

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- Number: US 10,865,524 B2
- Document ID: US10865524B2
- Status: Granted
- Kind: B2
- Application number: 16/387,019
- Filed: 2019-04-17
- Published: 2019-08-08
- Granted: 2020-12-15
- Earliest claimed: 2013-03-15
- Assignees: FiberLean Technologies Limited
- Applicants: FiberLean Technologies Limited
- Inventors: John Claude Husband; Per Svending
- Web page: https://patentgrep.com/patent/US10865524B2

## CPC

- D21H 17/74: {of organic and inorganic material}
- D21B 1/12: by wet methods, by the use of steam (beaters D21D1/00)
- D21D 1/30: Disc mills
- D21H 11/08: Mechanical or thermomechanical pulp
- D21H 11/18: Highly hydrated, swollen or fibrillatable fibres
- D21H 17/68: siliceous, e.g. clays
- D21H 21/18: Reinforcing agents
- D21H 11/10: Mixtures of chemical and mechanical pulp
- D21H 17/675: {Oxides, hydroxides or carbonates}
- D21H: PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21B: FIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
- D21D: TREATMENT OF THE MATERIALS BEFORE PASSING TO THE PAPER-MAKING MACHINE

## Abstract

A paper product may include high energy thermomechanical pulp (TMP), low energy TMP, and microfibrillated cellulose. The paper product may also include inorganic particulate material. A papermaking composition suitable for making the paper product, a process for preparing the paper product, and use of microfibrillated cellulose may include high energy TMP, low energy TMP, and microfibrillated cellulose, and optionally inorganic particulate material. The microfibrillated cellulose may have a fibre steepness of from about 20 to about 50 in the paper product.

## Claims

### Claim 1

A papermaking composition for preparing a paper product comprising high energy thermomechanical pulp (TMP), low energy TMP, and microfibrillated cellulose, and further comprising about 1% to about 50% by weight inorganic particulate material, wherein the paper product comprises at least about 30% by weight high energy TMP and low energy TMP and between 0.1% to 5% by weight of said microfibrillated cellulose, based on the total weight of the paper product; wherein the weight ratio of high energy TMP to low energy TMP is from about 55:45 to about 50:50; wherein the microfibrillated cellulose has a fibre steepness of from about 20 to about 50; wherein the low energy TMP has a Canadian standard freeness of from about 80 to about 130 cm3, and wherein the high energy TMP has a Canadian standard freeness of from 10 to 60 cm3.

### Claim 2 (depends on 1)

The papermaking composition of claim 1, wherein the microfibrillated cellulose is obtained by a process comprising microfibrillating a fibrous substrate comprising cellulose in an aqueous environment in the presence of a grinding medium.

### Claim 3 (depends on 2)

The papermaking composition of claim 2, wherein the microfibrillating the fibrous substrate comprising cellulose in an aqueous environment occurs in the presence of a grinding medium and inorganic particulate material.

### Claim 4 (depends on 1)

The papermaking composition of claim 1, wherein the inorganic particulate material is selected from the group consisting of at least one of an alkaline earth metal carbonate or sulphate, calcium carbonate, magnesium carbonate, dolomite, gypsum, a hydrous kandite clay, kaolin, halloysite, ball clay, anhydrous kandite clay, metakaolin, fully calcined kaolin, talc, mica, perlite, diatomaceous earth, magnesium hydroxide, aluminium trihydrate, and combinations thereof.

### Claim 5 (depends on 4)

The papermaking composition of claim 4, wherein the inorganic particulate material is kaolin.

### Claim 6 (depends on 5)

The papermaking composition of claim 5, wherein at least about 50% by weight of the kaolin has an equivalent spherical diameter of less than about 2 μm.

### Claim 7 (depends on 6)

The papermaking composition of claim 6, wherein the kaolin has at least one of a shape factor of from about 10 to about 70.