# US 10,864,491 B2 · Plant for producing a composition comprising drops and associated production process

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- Number: US 10,864,491 B2
- Document ID: US10864491B2
- Status: Granted
- Kind: B2
- Application number: 16/333,244
- Filed: 2017-09-13
- Published: 2019-08-15
- Granted: 2020-12-15
- Earliest claimed: 2016-09-14
- Assignees: Capsum
- Applicants: Capsum
- Inventors: Sébastien Bardon; Mathieu Goutayer; Yan Eric Pafumi
- Web page: https://patentgrep.com/patent/US10864491B2

## CPC

- B01F 33/844: {with means for customizing the mixture on the point of sale, e.g. by sensing, receiving or analysing information about the characteristics of the mixture to be made}
- A61K 8/03: Liquid compositions with two or more distinct layers
- A61K 8/11: Encapsulated compositions
- A61Q 13/00: Formulations or additives for perfume preparations (essential oils or perfumes per se C11B9/00)
- B01F 23/41: Emulsifying
- B01F 23/4105: {Methods of emulsifying}
- B01F 33/3011: using a sheathing stream of a fluid surrounding a central stream of a different fluid, e.g. for reducing the cross-section of the central stream or to produce droplets from the central stream
- B01F 23/4143: {Microemulsions}
- B01F 23/4145: {Emulsions of oils, e.g. fuel, and water}
- B01F 2101/21: Mixing of ingredients for cosmetic or perfume compositions
- B01F: MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING (mixing paints B44D3/06)
- A61K: PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES (devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms A61J3/00; chemical aspects of, or use of materials for deodorisation of air, for disinfection or sterilisation, or for bandages, dressings, absorbent pads or surgical articles A61L; soap compositions C11D)
- A61Q: SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS

## Abstract

The present invention relates to a plant (2) for producing a composition (9), in particular a cosmetic composition, comprising drops (8) of at least one first fluid dispersed in a second fluid substantially immiscible with the first fluid, each drop (8) comprising a core formed of the first fluid, and optionally a shell suitable for retaining the core, the plant (2) comprising: a device (16) for producing the composition (9), a storage module (10) comprising: at least one tank (36) for storing at least one first stock solution (A), and at least one tank (38) for storing at least one first solution of active agent(s), at least one tank (40) for storing at least one second stock solution (B), and a preparation module (12), connected to the storage module (10).

## Claims

### Claim 1

A plant for producing a composition, comprising drops of at least one first fluid dispersed in a second fluid that is substantially immiscible with the first fluid, wherein each drop comprises a core formed of the first fluid, wherein the plant comprises:
a device for producing the composition,
a storage module comprising:
at least one storage tank of at least a first stock solution, and at least one storage tank of at least a first solution of active agent(s) and/or additional compound(s), and
at least one storage tank of at least one second stock solution
a preparation module, connected to the storage module, designed to prepare at least:
the first fluid by mixing determined quantities of the first stock solution and at least the first solution of active agent(s) and/or additional compound(s), and
the second fluid by mixing determined quantities of the second stock solution,
wherein the preparation module is suitable for conveying in both a simultaneous manner and a sequential manner the first fluid and the second fluid in the production device,
a control unit designed to:
determine the quantity of one or more first solutions of active agents and/or additional compound(s) to be mixed with a determined quantity of the first stock solution to obtain the first fluid.

### Claim 2 (depends on 1)

The plant according to claim 1, wherein the storage module further comprises at least one storage tank of at least one perfume solution, wherein the preparation module is designed to add a determined quantity of the perfume solution(s), in the first fluid and/or in the second fluid and/or in the intermediate fluid.

### Claim 3 (depends on 1)

The plant according to claim 1, wherein the storage module comprises several tanks containing several first solutions of active agent(s) and/or additional compound(s), and/or several tanks containing several second solutions of active agent(s) and/or additional compound(s),
wherein the preparation module is able to mix selectively:
a determined quantity of one or more first solutions of active agent(s) and/or of additional compound(s) with a determined quantity of the first stock solution,
a determined quantity of one or more second solutions of active agent(s) and/or of additional compound(s) with a determined quantity of the second stock solution.

### Claim 4 (depends on 1)

The plant according to claim 1, wherein each storage tank of the storage module is removable.

### Claim 5 (depends on 1)

The plant according to claim 1, wherein the preparation module comprises selection valves of each solution to be mixed to obtain at least the first fluid, the second fluid, and, if appropriate, the intermediate fluid.

### Claim 6 (depends on 1)

The plant according to claim 1, wherein the preparation module comprises at least one static mixer, wherein each static mixer is designed to homogenize mixtures for forming the first fluid, the second fluid and/or, if appropriate, the intermediate fluid.

### Claim 7 (depends on 1)

The plant according to claim 1, wherein the production device comprises at least one element chosen from:
a nozzle
a mixer provided with at least one dispersion module, and
a static mixer.

### Claim 8 (depends on 7)

The plant according to claim 7, wherein the production device comprises at least a plurality of nozzles, wherein first rails and second rails, and, where appropriate, third rails, are each connected to the plurality of nozzles, wherein the nozzles are preferably arranged in parallel with each other.

### Claim 9 (depends on 7)

The plant according to claim 7, wherein each distribution rail is connected to the corresponding nozzle by a connection forming a pressure drop.

### Claim 10 (depends on 1)

The plant according to claim 1, wherein the plant comprises a collector connected to the production device and capable of collecting the composition.

### Claim 11 (depends on 10)

The plant according to claim 10, wherein the production device and/or the collector comprises at least one injection device of a solution for increasing the viscosity of the second fluid.

### Claim 12 (depends on 11)

The plant according to claim 11, wherein a rail for distribution of a solution for increasing the viscosity is connected to each nozzle in order to inject the solution for increasing viscosity in the second fluid after the formation of drops.

### Claim 13 (depends on 1)

A method for producing a composition, comprising drops of at least one first fluid dispersed in a second fluid that is substantially immiscible with the first fluid, wherein each drop comprises a core formed of the first fluid from a plant according to claim 1, wherein the method comprises:
the preparation, in the preparation module:
of the first fluid by mixing determined quantities of the first stock solution and at least a first solution of active agent(s) and/or additional compound(s), and
of the second fluid by mixing determined quantities of the second stock solution,
the simultaneous or sequential conveying of the first fluid, the second fluid and, if appropriate, the intermediate fluid in the production device, and
the formation of a composition by the production device.

### Claim 14 (depends on 13)

The method according to claim 13, wherein the method further comprises, after the step of forming the composition:
the preparation in the same preparation module of at least one additional fluid different from the first fluid and/or of at least one second additional fluid different from the second fluid, and
the simultaneous or sequential conveying of the first additional fluid, the second additional fluid, and
the formation of an additional composition by the production device.

### Claim 15 (depends on 13)

The method according to claim 13, wherein the method further comprises, after the step of forming the composition, a step of injecting a solution for increasing the viscosity of the composition, especially the second fluid.

### Claim 16 (depends on 14)

A process of personalizing a composition by a consumer, comprising a step of using the plant according to claim 14.

### Claim 17 (depends on 7)

The plant according to claim 7, wherein the nozzle comprises a hollow body delimiting an internal duct and an external duct extending along a vertical longitudinal axis and arranged in a coaxial manner along the longitudinal axis, wherein the external duct opens downwards through an opening forming drops,
wherein the nozzle comprises a first external feed duct of the first fluid and a second external feed duct of the second fluid,
wherein the first external feed duct is connected to the internal duct, while the second external feed duct is connected to the external duct.

### Claim 18 (depends on 1)

The plant according to claim 1, wherein each drop comprises a shell that is designed to retain the core,
wherein the storage module comprises at least one storage tank of at least a third stock solution,
wherein the preparation module is designed to prepare an intermediate fluid by mixing determined quantities of the third stock solution,
wherein the preparation module is suitable for conveying, the intermediate fluid.

### Claim 19 (depends on 18)

The plant according to claim 18, wherein the storage module further comprises, at least one storage tank of at least one third solution of active agent(s) and/or additional compound(s),
wherein the preparation module is designed to prepare the intermediate fluid by mixing, determined quantities of the third stock solution and of at least the third solution of active agent(s) and/or additional compound(s), and
wherein the control unit is designed to determine the quantity of the third stock solution to be mixed with a determined quantity of one or more third solutions of active agent(s) and/or additional compound(s) to obtain the intermediate fluid.

### Claim 20 (depends on 1)

The plant according to claim 1, wherein the storage module further comprises at least one storage tank of at least one second solution of active agent(s) and/or additional compound(s),
wherein the preparation module is designed to prepare the second fluid by mixing, determined quantities of the second stock solution and of at least the second solution of active agent(s) and/or additional compound(s), and
wherein the control unit is designed to determine the quantity of one or more second solutions of active agent(s) and/or additional compound(s) to be mixed with the determined quantity of the second stock solution to obtain the second fluid.

### Claim 21 (depends on 3)

The plant according to claim 3, wherein the storage module comprises several tanks containing several perfume solutions, and wherein the preparation module is able to mix selectively a determined quantity of one or more perfume solutions(s) to form the first fluid and/or the second fluid.

### Claim 22 (depends on 21)

The plant according to claim 21, wherein the storage module comprises several tanks containing several third solutions of active agent(s) and/or additional compound(s), and wherein the preparation module is able to mix selectively a determined quantity of one or more third solutions of active agent(s) and/or of additional compound(s) with a determined quantity of third stock solution and a determined quantity of one or several perfume solutions for forming the intermediate fluid.

### Claim 23 (depends on 17)

The plant according to claim 17, wherein the nozzle further comprises a third external feed duct of the intermediate fluid, connected to the internal duct.
