Method of producing apatite crystal, and apatite crystal
AssigneeKoito Manufacturing Co., Ltd.
InventorsYu Shinomiya, Kazumichi Yanagisawa, Masoud Sakaki
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Abstract
A method of producing an apatite crystal includes the steps of preparing an apatite single crystal expressed by the general formula M25(PO4)3X (M2 being at least atomic element selected from the group consisting of divalent alkaline-earth metals and Eu, and X is at least one atomic selected from the group consisting of halogens); placing the apatite single crystal into a space controllable to a predetermined atmosphere; supplying water vapor into the space; and heating such that the atmosphere in the space is within a 1000° C. to 1400° C. range.
Claims2
A method of producing an apatite crystal, the method comprising:
- preparing a tubular apatite single crystal expressed by the general formula M25(PO4)3X, wherein M2 is at least one atomic element selected from the group consisting of divalent alkaline-earth metals and Eu, and X is at least one atomic element selected from the group consisting of halogens;
- placing the apatite single crystal into a space controllable to a predetermined atmosphere;
- supplying water vapor into the space:
- and
- heating such that the atmosphere in the space is at a temperature at which a portion of the halogen atoms contained in the apatite single crystal are replaced with hydroxyl groups,
- wherein the step of heating is carried out within a 6 to 24 hour range, and
- wherein in the step of heating, the heating is such that the atmosphere in the space is in the range of 1100° C. to 1200° C.
Dependencies are inferred from the claim text.