Back to results
US 10,752,731 B2Granted
Process for the continuous production of polyether polyols
AssigneesBASF SE, BASF Schwarzheide GmbH
InventorsJulia Grosse-Willerich, Kerstin Wiss, Karl-Heinz Wassmer, Peter Deglmann, Christian Buss, Vinit Chilekar
Life of this patent
Estimating the term…
Abstract
This invention relates to a process for the continuous production of polyether polyols, polyether polyols produced by the inventive continuous process and their use in polyurethane applications.
Claims2
A process for continuous production of polyether alcohols, the process comprising:
- (a) continuously adding at least one aromatic amine (AA) at one dosing point D1 to an arrangement R1 comprising at least one plug-flow reactor (PFR) and/or a cascade of at least two continuously stirred tank reactors (CSTRs), and reacting with at least one alkylene oxide 1 (AO1) which is continuously dosed into the arrangement R1 at one or more dosing points D2 to generate an intermediate (I);
- and subsequently
- (b) continuously transferring the intermediate (I) into another arrangement R2 comprising at least one further reactor, and reacting with at least one alkylene oxide 2 (AO2) in the presence of at least one amine compound (AC), wherein at least one of the at least one amine compounds AC is selected from the group consisting of imidazoles, wherein the transferring (b) is initiated when the amount of free aromatic amine (AA) in the adding (a), as determined by gas chromatography, is less than 2% by weight, in relation to the total amount of the intermediate.
Dependencies are inferred from the claim text.