MAS NMR probe head arrangement with replaceable stator
AssigneeBruker Switzerland AG
InventorsNicolas Freytag, Fabian Kuehler, David Osen
Life of this patent
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Abstract
An MAS NMR probe head arrangement has a stator (2) aligned along an axis of rotation (RA) to support a rotor (1), a stator mount (32), and a RF coil arrangement (21) to emit/receive RF pulses into/from the measurement substance (40) in the rotor. The stator mount has a stator bearing (41) into which the stator can be axially inserted and extracted. The stator, when inserted, passes through the RF coil arrangement (21), and can be fed through the RF coil arrangement (21). A mechanism fixes the stator axially in the stator bearing (41) when inserted. This arrangement enhances both ease of assembly and maintenance of the arrangement.
Claims22
A magic angle spinning (MAS) nuclear magnetic resonance (NMR) probe head arrangement, comprising:
- a stator aligned along an axis of rotation and configured to support a rotor holding a measurement substance,
- a stator mount,
- a radio frequency (RF) coil arrangement configured to emit RF pulses into the measurement substance held in the rotor and/or to receive RF signals from the measurement substance held in the rotor, and
- a mechanism,
- wherein the stator comprises a first bearing base, a sleeve element, and a second bearing base, wherein the sleeve element connects the first bearing base and the second bearing base to each other axially as a unit, wherein the first bearing base is configured as a first pneumatic bearing and the second bearing base is configured as a second pneumatic bearing,
- wherein the second bearing base has a greatest external diameter AD2,
- wherein the sleeve element has a frontal section which adjoins the second bearing base axially and has a greatest external diameter ADV,
- wherein the RF coil arrangement has a least inner diameter IDS,
- wherein:
- AD2<IDS and ADV<IDS,
- wherein the stator mount is formed with a stator bearing configured for axial insertion and axial extraction of the stator as the unit into and from the stator mount,
- wherein the stator is configured to pass through the RF coil arrangement for axial insertion into and axial extraction from the stator mount, and
- wherein the mechanism is configured to fix the stator axially in the stator bearing when the stator is inserted into the stator mount.
Dependencies are inferred from the claim text.