Polyarylene sulfide production method and polyarylene sulfide
AssigneeKureha Corporation
InventorsAkihiro Konno, Ken-Ichi Takaki, Yui Yoshida, Hiroyuki Sato
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AssigneeKureha Corporation
InventorsAkihiro Konno, Ken-Ichi Takaki, Yui Yoshida, Hiroyuki Sato
Estimating the term…
A method of producing a polyarylene sulfide (PAS) includes a preparation step of preparing a charged mixture containing an organic amide solvent, a sulfur source, water, and a dihalo aromatic compound; a first-stage polymerization step of performing a polymerization reaction on the charged mixture at a temperature of from 170 to 280° C. to produce a prepolymer having a conversion ratio of the dihalo aromatic compound of 50% or greater; and a second-stage polymerization step of continuing the polymerization reaction in a phase-separated state at a temperature of from 245 to 290° C. in a reaction system containing the prepolymer, and includes adding a polyfunctional compound to the reaction system in the phase-separated state. A PAS having a melt viscosity (310° C., shear rate: 1216 sec−1) of from 0.1 to 8000 Pa·s is produced by the method.
A method of producing a polyarylene sulfide comprising:
Dependencies are inferred from the claim text.