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US 10,626,523 B2Granted
Fiber and a process for the manufacture thereof
AssigneeStora Enso OYJ
InventorsNiklas Garoff, Robert Protz, Jens Erdmann, Johnannes Ganster, André Lehmann
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Abstract
The present invention relates to a method for manufacturing thermally stabilized, non-sticky and stretchable fibers, which may be further processed into intermediate carbon fibers and finally also carbon fibers. Uses of said fibers are also disclosed. Also a highly oriented intermediate carbon fiber is disclosed together with a highly oriented carbon fiber.
Claims14
A method for manufacturing a highly oriented intermediate carbon fiber, comprising the following steps:
- a. providing cellulose and/or a cellulose derivative,
- b. providing lignin and/or a lignin derivative,
- c. dissolution of the cellulose and/or cellulose derivative and the lignin and/or lignin derivative followed by subsequent mixing thus providing a dope,
- d. performing a solution spinning of the dope to a precursor material,
- e. performing a stabilization on the precursor material at a temperature from about 100 to about 450° C. at a residence time of from 10 to 180 minutes, thus providing a thermally stabilized, non-sticky and stretchable fiber, and
- f. performing a stretch-pre-carbonization, including stretching and pre-carbonization, on the thermally stabilized, non-sticky and stretchable fiber at temperatures from about 200 to about 1300° C., thus providing a highly oriented intermediate carbon fiber,
- wherein said stretching is carried out at elongations between 25% and 1000%.
4 more elements
Dependencies are inferred from the claim text.