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US 10,619,102 B2Granted
High temperature bio-char carbonization and micron grinding and classification for inclusion into master batch polymerization
AssigneeThomas Jefferson University
InventorMark Sunderland
Life of this patent
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Abstract
A thermal process for carbonizing hemp and reducing particle size, mechanically, by grinding or milling said carbonized hemp materials to generate a precise particle size hemp char and combining the hemp char particles with a polymer into a master batch.
Claims21
A process for creating a mixture of micron-sized charred hemp comprising:
- rough cutting a portion of hemp stalk, said portion of hemp stalk comprising fiber and hurd materials;
- charring the portion of hemp stalk at a temperature of greater than 1100° Celsius to create a char material;
- milling the char material to create a milled char;
- classifying the milled char with a classification system of less than 10 micron size to create a fraction of hemp char particles;
- collecting a desired fraction from the classification system of hemp char particles of less than 10 microns in size.
2 more elements
A process for creating a masterbatch comprising a plurality of hemp char particles and a polymer comprising:
- carbonizing a portion of a hemp material in a furnace, said portion of hemp material comprising hemp fiber and hurd, said furnace being flushed with nitrogen and then heated to greater than 1100° C.;
- wherein the temperature greater than 1100° C. is held for at least 60 minutes;
- nitrogen flow is maintained over the at least 60 minutes to maintain a low oxygen environment to create a char;
- removing the char from the furnace and allowing it to cool;
- milling the char by a milling process for a period sufficient to reduce the char into a plurality of particles having average particle size of less than 2 microns to create char particles of less than 2 microns;
- combining the char particles having an average particle size of less than 2 microns with the polymer, wherein the ratio of char particles to polymer is between 10:90 and 50:50;
- and mixing the polymer and the char particles to form the masterbatch.
4 more elements
A process of forming charred hemp particles of less than 2 micron in size, comprising:
- drying cut hemp stalk on a field for a period of less than 7 days, said hemp stalk comprising fiber and hurd;
- pyrolyzing the dried hemp stalk at 1100°-1500° Celsius to create a char;
- adding the char to a grinding vessel and grinding the char for a period of 1 to 16 hours;
- screening the ground char with a 2 micron screen to create a screened char of less than 2 microns;
- and capturing the screened char of less than 2 microns.
2 more elements
Dependencies are inferred from the claim text.