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US 10,563,918 B2Granted
Lithium stuffed garnet setter plates for solid electrolyte fabrication
AssigneeQuantumScape Corporation
InventorsSriram Iyer, Tim Holme, Niall Donnelly
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Abstract
Setter plates are fabricated from Li-stuffed garnet materials having the same, or substantially similar, compositions as a garnet Li-stuffed solid electrolyte. The Li-stuffed garnet setter plates, set forth herein, reduce the evaporation of Li during a sintering treatment step and/or reduce the loss of Li caused by diffusion out of the sintering electrolyte. Li-stuffed garnet setter plates, set forth herein, maintain compositional control over the solid electrolyte during sintering when, upon heating, lithium is prone to diffuse out of the solid electrolyte.
Claims13
A slurry comprising:
- lithium-stuffed garnet characterized by the formula LiALaBM′CM″DZrEOF, wherein 4<A<8.5, 1.5<B<4, 0≤C≤2, 0≤D≤2;
- 0≤E<2, 10<F<13, and M′ and M″ are each, independently in each instance, selected from Al, Mo, W, Nb, Sb, Ca, Ba, Sr, Ce, Hf, Rb, and Ta;
- an acrylic binder;
- and
- benzyl butyl phthalate;
- wherein the benzyl butyl phthalate is present at 5% w/w.
3 more elements
Dependencies are inferred from the claim text.